Studying the Structure and Mechanical Properties of AlN–С–TiB2 Ceramic Composites

IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY
T. B. Serbeniuk, T. O. Prikhna, V. B. Sverdun, V. E. Moshchil, M. V. Karpets, A. A. Marchenko, V. V. Bilorusets, S. P. Starik
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Abstract

The structure formation features and mechanical properties of the AlN–С–TiB2 ceramic composite containing 2 wt % of diamond powder and 13 wt % of TiB2 for vacuum electronics applications were investigated. Composite samples were sintered by hot pressing at a temperature 1900°C and a pressure of 20 MPa. Using structural and X-ray diffraction studies, the AlN, Al3(O, N)4, TiB2, TiC, Y3Al5O12, and C (graphite) phases were revealed in the material. When measuring the mechanical properties, it was found that the Vickers hardness of the studied composite materials is 12.5 ± 0.44 GPa at a load on the indenter of 9.8 N. Increasing the indenter load to 49 N led to the formation of cracks, and the fracture toughness under such conditions was 5.82 ± 0.11 MPa m0.5.

AlN -С-TiB2陶瓷复合材料的结构与力学性能研究
研究了真空电子用金刚石粉含量为2 wt %、TiB2含量为13 wt %的AlN -С-TiB2陶瓷复合材料的结构、形成特征和力学性能。在温度1900℃,压力20 MPa的条件下进行热压烧结。通过结构和x射线衍射分析,发现材料中存在AlN、Al3(O, N)4、TiB2、TiC、Y3Al5O12和C(石墨)相。在力学性能测试中发现,在压头载荷为9.8 N时,复合材料的维氏硬度为12.5±0.44 GPa,当压头载荷增加到49 N时,导致裂纹的形成,该条件下的断裂韧性为5.82±0.11 MPa m0.5。
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来源期刊
Journal of Superhard Materials
Journal of Superhard Materials MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
1.80
自引率
66.70%
发文量
26
审稿时长
2 months
期刊介绍: Journal of Superhard Materials presents up-to-date results of basic and applied research on production, properties, and applications of superhard materials and related tools. It publishes the results of fundamental research on physicochemical processes of forming and growth of single-crystal, polycrystalline, and dispersed materials, diamond and diamond-like films; developments of methods for spontaneous and controlled synthesis of superhard materials and methods for static, explosive and epitaxial synthesis. The focus of the journal is large single crystals of synthetic diamonds; elite grinding powders and micron powders of synthetic diamonds and cubic boron nitride; polycrystalline and composite superhard materials based on diamond and cubic boron nitride; diamond and carbide tools for highly efficient metal-working, boring, stone-working, coal mining and geological exploration; articles of ceramic; polishing pastes for high-precision optics; precision lathes for diamond turning; technologies of precise machining of metals, glass, and ceramics. The journal covers all fundamental and technological aspects of synthesis, characterization, properties, devices and applications of these materials. The journal welcomes manuscripts from all countries in the English language.
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