Synthesis and structure of a 1:1 cocrystal of N,N′-bis­(pyridin-3-ylmeth­yl)pyromellitic di­imide and naphthalene-2,6-di­carb­oxy­lic acid

IF 0.5 Q4 CRYSTALLOGRAPHY
Luccile Mbonzhe, Eustina Batisai
{"title":"Synthesis and structure of a 1:1 cocrystal of N,N′-bis­(pyridin-3-ylmeth­yl)pyromellitic di­imide and naphthalene-2,6-di­carb­oxy­lic acid","authors":"Luccile Mbonzhe,&nbsp;Eustina Batisai","doi":"10.1107/S2056989026006110","DOIUrl":null,"url":null,"abstract":"<div><div>In the title cocrystal, C<sub>22</sub>H<sub>14</sub>N<sub>4</sub>O<sub>4</sub>·C<sub>12</sub>H<sub>8</sub>O<sub>4</sub>, both components are completed by crystallographic inversion symmetry and the dihedral angle between the central fused ring system and the pendant pyridine ring is 66.21 (5)°. In the extended structure, the components are linked by O—H⋯N hydrogen bonds, generating [001] chains, and the packing is consolidated by π–π stacking and C—H⋯O inter­actions.</div></div>","PeriodicalId":7367,"journal":{"name":"Acta Crystallographica Section E: Crystallographic Communications","volume":"82 7","pages":"Pages 854-857"},"PeriodicalIF":0.5000,"publicationDate":"2026-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Crystallographica Section E: Crystallographic Communications","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S2056989026001647","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2026/7/13 0:00:00","PubModel":"Epub","JCR":"Q4","JCRName":"CRYSTALLOGRAPHY","Score":null,"Total":0}
引用次数: 0

Abstract

In the title cocrystal, C22H14N4O4·C12H8O4, both components are completed by crystallographic inversion symmetry and the dihedral angle between the central fused ring system and the pendant pyridine ring is 66.21 (5)°. In the extended structure, the components are linked by O—H⋯N hydrogen bonds, generating [001] chains, and the packing is consolidated by π–π stacking and C—H⋯O inter­actions.
N,N'-二-(吡啶-3-基甲基)二酰亚胺与萘-2,6-二碳水化合物氧酸1:1共晶的合成与结构
在题目共晶C22H14N4O4·C12H8O4中,两组分均通过晶体倒置对称完成,中心熔合环体系与悬垂吡啶环之间的二面角为66.21(5)°。在扩展结构中,组分通过O- h⋯N氢键连接,产生[001]链,并且包装通过π-π堆叠和C-H⋯O相互作用来巩固。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
求助全文
约1分钟内获得全文 求助全文
来源期刊
CiteScore
1.90
自引率
0.00%
发文量
351
审稿时长
3 weeks
期刊介绍: Acta Crystallographica Section E: Crystallographic Communications is the IUCr''s open-access structural communications journal. It provides a fast, simple and easily accessible publication mechanism for crystal structure determinations of inorganic, metal-organic and organic compounds. The electronic submission, validation, refereeing and publication facilities of the journal ensure rapid and high-quality publication of fully validated structures. The primary article category is Research Communications; these are peer-reviewed articles describing one or more structure determinations with appropriate discussion of the science.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信
小红书