The Effect of PTFE Coating and PTFE Tape Wrapping Abutment Screw After Cyclic Loading: An In Vitro Study.

IF 4
Poonnarat Kongkhuntian, Weerapan Aunmeungtong, Pathawee Khongkhunthian
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Abstract

Objective: This study aimed to compare the effect of PTFE tape wrapping and PTFE-coated titanium alloy screws on the removal torque after cyclic loading and on preload values under repetitive tightening.

Methods: A total of 60 titanium abutment screws were allocated to three surface-treatment groups (n = 20 each): untreated (Control), PTFE tape-wrapped (Wrap), and PTFE-coated (Coat). Within each group, 10 specimens underwent cyclic loading, whereas 10 were assigned to preload evaluation. Cyclic loading followed ISO 14801:2016. Screws were tightened to 30 N·cm, retightened after 10 min, and subjected to 300 000 cycles at 200 N using a fatigue testing machine (DYNA-MESS Prüfsysteme GmbH, Aachen, Germany). Removal torque was measured with a digital torque gauge (BTGE50CN, Tohnichi, Japan). For preload assessment, each specimen completed 10 tightening-loosening cycles at the same torque during which tensile force was recorded using a customized device. One representative screw per group was analyzed by SEM and micro-CT before and after loading to evaluate surface and structural changes.

Results: After cyclic loading, the removal torque did not differ significantly between the Control group (17.58 ± 1.85 N·cm) and the Wrap group (17.50 ± 1.77 N·cm), whereas the Coat group demonstrated significantly lower removal torque (14.71 ± 2.35 N·cm; p < 0.05). In the preload test, preload progressively decreased in the Control (-3.13 N per cycle) and Coat groups (-0.51 N per cycle), while the Wrap group showed a consistent increase with repeated tightening (+8.22 N per cycle). SEM revealed surface wear and partial loss of PTFE material after loading, particularly in the coated specimens. Micro-CT analysis showed no detectable differences in internal adaptation among groups before or after cyclic loading.

Conclusions: PTFE tape wrapping increased preload during repeated tightening but did not improve removal torque after cyclic loading compared with those of untreated screws. Although PTFE-coated screws produced the highest initial preload, they were associated with reduced removal torque after loading. SEM analysis confirmed coating deterioration, whereas internal fit remained comparable across groups.

聚四氟乙烯涂层和聚四氟乙烯胶带包绕基牙螺钉循环加载后的体外研究。
目的:比较聚四氟乙烯(PTFE)带包覆和PTFE涂层钛合金螺钉对循环加载后取下扭矩和重复拧紧预紧力值的影响。方法:将60枚钛基牙螺钉分为3个表面处理组(n = 20):未处理组(Control)、PTFE胶带包覆组(Wrap)和PTFE涂层组(Coat)。在每组中,10个试件进行循环加载,10个试件进行预加载评估。循环加载遵循ISO 14801:2016。将螺钉拧紧至30 N·cm, 10分钟后重新拧紧,并使用疲劳试验机(DYNA-MESS profsysteme GmbH, Aachen, Germany)在200 N下进行30万次循环。用数字式扭矩计(BTGE50CN, Tohnichi, Japan)测量拆卸扭矩。对于预加载评估,每个试件在相同扭矩下完成10个拧紧-松开循环,在此期间使用定制的设备记录拉伸力。每组各1颗代表性螺钉在加载前后通过SEM和micro-CT分析其表面和结构变化。结果:循环加载后,Control组(17.58±1.85 N·cm)与Wrap组(17.50±1.77 N·cm)的去除扭矩无显著差异,而Coat组的去除扭矩显著降低(14.71±2.35 N·cm); p结论:与未处理的螺钉相比,PTFE胶带缠绕在重复拧紧过程中增加了预紧力,但没有改善循环加载后的去除扭矩。尽管ptfe涂层螺钉产生了最高的初始预载荷,但它们与加载后的移除扭矩降低有关。扫描电镜分析证实涂层恶化,而内部配合在各组之间保持可比性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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