Synthesis and structural analysis of novel bisallenylphosphoramide derivatives

IF 2.4 Q2 Chemistry

Chemical Data Collections Pub Date : 2026-03-01 Epub Date: 2026-02-12 DOI:10.1016/j.cdc.2026.101230

K. Abaid , C. Ben Aissa , N. Jebli , K. Van Hecke , S. Touil

引用次数: 0

Abstract

A series of unprecedented bisallenylphosphoramides was prepared using a two-step synthetic pathway from terminal propargyl alcohols. The structures of the synthesized compounds were characterized by various spectroscopic tools including IR, NMR (¹H, ³¹P, ¹³C), as well as mass spectrometry and single-crystal X-ray diffraction. Intermolecular interactions in the crystal structure were further studied and confirmed using Hirshfeld surface analysis.

Abstract Image

查看原文本刊更多论文

新型双烯基磷酰胺衍生物的合成及结构分析

以端丙炔醇为原料，采用两步法合成了一系列前所未有的双烯基磷酰胺。用红外光谱、核磁共振（1H、31P、13C）、质谱和x -射线单晶衍射等手段对合成化合物的结构进行了表征。利用Hirshfeld表面分析进一步研究了晶体结构中的分子间相互作用。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

求助全文

约1分钟内获得全文求助全文

来源期刊

Chemical Data Collections Chemistry-Chemistry (all)

CiteScore

6.10

自引率

0.00%

发文量

169

审稿时长

24 days

期刊介绍： Chemical Data Collections (CDC) provides a publication outlet for the increasing need to make research material and data easy to share and re-use. Publication of research data with CDC will allow scientists to: -Make their data easy to find and access -Benefit from the fast publication process -Contribute to proper data citation and attribution -Publish their intermediate and null/negative results -Receive recognition for the work that does not fit traditional article format. The research data will be published as ''data articles'' that support fast and easy submission and quick peer-review processes. Data articles introduced by CDC are short self-contained publications about research materials and data. They must provide the scientific context of the described work and contain the following elements: a title, list of authors (plus affiliations), abstract, keywords, graphical abstract, metadata table, main text and at least three references. The journal welcomes submissions focusing on (but not limited to) the following categories of research output: spectral data, syntheses, crystallographic data, computational simulations, molecular dynamics and models, physicochemical data, etc.