3-(4-Ethynylphenyl)-1,5-diphenylformazan

Molbank Pub Date : 2025-03-03 DOI:10.3390/m1976

Ida A. Lupanova, Dzhamilya N. Konshina, I. V. Sukhno, Ekaterina S. Spesivaya, В. В. Коншин

引用次数: 1

Abstract

The structure of the “clickable” formazan, 3-(4-ethynylphenyl)-1,5-diphenylformazan, has been determined for the first time in a single crystal. The synthesis of 3-(4-ethynylphenyl)-1,5-diphenylformazan was carried out by coupling 4-(trimethylsilyl)ethynylbenzaldehyde phenylhydrazone with diazotized aniline, followed by desilylation, with a total yield of 54%.

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(3) - 4-Ethynylphenyl 5-diphenylformazan

“可点击”的3-（4-乙基苯基）-1,5-二苯基甲醛的结构首次在单晶中被确定。采用4-（三甲基硅基）乙基苯甲醛苯腙与重氮苯胺偶联，再进行脱硅反应，合成了3-（4-乙基苯基）-1,5-二苯基甲氮酮，总收率为54%。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊