Effects of laser cutting and post-processing on the microstructure and properties of thin sintered Nd-Fe-B magnets

IF 3 3区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY
Lichun Zhan , Wenyu Pan , Ruihua Du , Weiqiang Liu , Zan Long , Shengli Jia , Qifeng Wei , Xiongfei Wu , Ming Yue
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引用次数: 0

Abstract

Laser cutting, recognized for its narrow kerf, high efficiency, and adaptability to complex geometries, is increasingly employed in the machining of thin sintered Nd–Fe–B magnets. This work systematically evaluates the influence of laser cutting versus conventional multi-wire cutting combined with grinding on the microstructure, mechanical strength, and magnetic properties of magnets under black, chamfered, and pickled conditions. Laser cutting induces stepped demagnetization curves, lowers intrinsic coercivity and mechanical properties compared to conventional multi-wire cutting combined with grinding method. Results indicate that chamfering improves the three-point bending force of laser-cut samples by approximately 31.4% on average. After pickling, the specific magnetic moment of laser-cut samples is only 0.13% lower, and the irreversible flux loss is merely 0.08% higher than that of ground specimens. Microstructural analysis reveals that laser-cut surfaces contain a resolidified layer, micropores, and networked microcracks, which contribute to the degradation in mechanical and magnetic properties. Magnetic domain observations further demonstrate that laser-cut black samples exhibit blurred domain boundaries and maze domains, whereas chamfered specimens show a marked reduction in maze domains and improved domain alignment. Under identical reverse magnetic fields, domain reversal occurs more readily in black samples than in chamfered ones. In summary, through appropriate parameter selection and post-processing, such as chamfering and pickling, the mechanical and magnetic performance of laser-cut thin Nd-Fe-B magnets can closely match that of ground magnets, offering valuable guidance for process optimization in thin magnet manufacturing.
激光切割和后处理对烧结Nd-Fe-B薄磁体组织和性能的影响
激光切割以其窄切口、高效率和对复杂几何形状的适应性而被越来越多地应用于烧结钕铁硼薄磁体的加工。本研究系统地评估了在黑色、倒角和酸洗条件下,激光切割与传统多线切割结合磨削对磁体微观结构、机械强度和磁性能的影响。激光切割产生阶梯退磁曲线,与传统的多线切割结合磨削方法相比,具有较低的内在矫顽力和力学性能。结果表明,倒角可使激光切割样品的三点弯曲力平均提高约31.4%。经酸洗处理后,激光切割样品的比磁矩仅比地面样品低0.13%,不可逆磁通量损失仅比地面样品高0.08%。显微结构分析表明,激光切割表面含有再凝固层、微孔和网状微裂纹,这些都导致了机械性能和磁性能的下降。磁畴观察进一步表明,激光切割的黑色样品显示出模糊的畴边界和迷宫畴,而倒角样品显示出迷宫畴的显著减少和改进的畴对齐。在相同的反向磁场下,黑色样品比倒角样品更容易发生畴反转。综上所述,通过适当的参数选择和倒角、酸洗等后处理,激光切割的Nd-Fe-B薄磁体的机械性能和磁性能可以与地面磁体的机械性能和磁性能接近,为薄磁体制造的工艺优化提供了有价值的指导。
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来源期刊
Journal of Magnetism and Magnetic Materials
Journal of Magnetism and Magnetic Materials 物理-材料科学:综合
CiteScore
5.30
自引率
11.10%
发文量
1149
审稿时长
59 days
期刊介绍: The Journal of Magnetism and Magnetic Materials provides an important forum for the disclosure and discussion of original contributions covering the whole spectrum of topics, from basic magnetism to the technology and applications of magnetic materials. The journal encourages greater interaction between the basic and applied sub-disciplines of magnetism with comprehensive review articles, in addition to full-length contributions. In addition, other categories of contributions are welcome, including Critical Focused issues, Current Perspectives and Outreach to the General Public. Main Categories: Full-length articles: Technically original research documents that report results of value to the communities that comprise the journal audience. The link between chemical, structural and microstructural properties on the one hand and magnetic properties on the other hand are encouraged. In addition to general topics covering all areas of magnetism and magnetic materials, the full-length articles also include three sub-sections, focusing on Nanomagnetism, Spintronics and Applications. The sub-section on Nanomagnetism contains articles on magnetic nanoparticles, nanowires, thin films, 2D materials and other nanoscale magnetic materials and their applications. The sub-section on Spintronics contains articles on magnetoresistance, magnetoimpedance, magneto-optical phenomena, Micro-Electro-Mechanical Systems (MEMS), and other topics related to spin current control and magneto-transport phenomena. The sub-section on Applications display papers that focus on applications of magnetic materials. The applications need to show a connection to magnetism. Review articles: Review articles organize, clarify, and summarize existing major works in the areas covered by the Journal and provide comprehensive citations to the full spectrum of relevant literature.
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