Texture control in new biomedical Nb30Ti30Zr30Cr5Mo5 medium entropy alloy through high temperature uniaxial compression for Young's modulus reduction

IF 5.3 2区材料科学 Q2 CHEMISTRY, PHYSICAL

Intermetallics Pub Date : 2026-01-01 Epub Date: 2025-11-03 DOI:10.1016/j.intermet.2025.109062

Pramote Thirathipviwat , Ryota Muraki , Wakaba Onuki , Daichi Minami , Jithin Vishnu , Ansheed Raheem , Kesavan Praveenkumar , Geetha Manivasagam , Equo Kobayashi , Makoto Hasegawa

{"title":"Texture control in new biomedical Nb30Ti30Zr30Cr5Mo5 medium entropy alloy through high temperature uniaxial compression for Young's modulus reduction","authors":"Pramote Thirathipviwat , Ryota Muraki , Wakaba Onuki , Daichi Minami , Jithin Vishnu , Ansheed Raheem , Kesavan Praveenkumar , Geetha Manivasagam , Equo Kobayashi , Makoto Hasegawa","doi":"10.1016/j.intermet.2025.109062","DOIUrl":null,"url":null,"abstract":"<div><div>In this study, we investigate the potential of texture control for preferred {001} orientation to reduce the Young's modulus in the new biomedical body-centered cubic (BCC) Nb30Ti30Zr30Cr5Mo5 MEA. The fabrication of {001} oriented grains on a compression plane is controlled by so-called preferential dynamic grain growth under high temperature uniaxial compression. The uniaxial compression is carried out at temperature between 1073 and 1473 K by a true strain rate between 1 × 10−4 – 1 × 10−2 s−1 until −1.0 in true strain. The microstructures after the compression at 1473 K are significantly developed by dynamic recrystallization. A decrease in true strain rate promotes a formation of {001} oriented grains due to enhanced preferential dynamic grain growth. The highest volume fraction of {001} texture (∼64 %) is observed after the compression at 1473 K under the strain rate of 5.0 × 10−4 s−1. An increase in volume fraction of {001} texture decrease the Young's modulus. The Young's modulus in this study can reduce as low as 68 GPa, compared with ∼93 GPa in the initial sample prior to high-temperature deformation.</div></div>","PeriodicalId":331,"journal":{"name":"Intermetallics","volume":"188 ","pages":"Article 109062"},"PeriodicalIF":5.3000,"publicationDate":"2026-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Intermetallics","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0966979525004273","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"2025/11/3 0:00:00","PubModel":"Epub","JCR":"Q2","JCRName":"CHEMISTRY, PHYSICAL","Score":null,"Total":0}

引用次数: 0

Abstract

In this study, we investigate the potential of texture control for preferred {001} orientation to reduce the Young's modulus in the new biomedical body-centered cubic (BCC) Nb₃₀Ti₃₀Zr₃₀Cr₅Mo₅ MEA. The fabrication of {001} oriented grains on a compression plane is controlled by so-called preferential dynamic grain growth under high temperature uniaxial compression. The uniaxial compression is carried out at temperature between 1073 and 1473 K by a true strain rate between 1 × 10⁻⁴ – 1 × 10⁻² s⁻¹ until −1.0 in true strain. The microstructures after the compression at 1473 K are significantly developed by dynamic recrystallization. A decrease in true strain rate promotes a formation of {001} oriented grains due to enhanced preferential dynamic grain growth. The highest volume fraction of {001} texture (∼64 %) is observed after the compression at 1473 K under the strain rate of 5.0 × 10⁻⁴ s⁻¹. An increase in volume fraction of {001} texture decrease the Young's modulus. The Young's modulus in this study can reduce as low as 68 GPa, compared with ∼93 GPa in the initial sample prior to high-temperature deformation.

查看原文本刊更多论文

通过高温单轴压缩降低杨氏模量来控制新型生物医用Nb30Ti30Zr30Cr5Mo5中熵合金的织构

在这项研究中，我们研究了优选{001}取向的织构控制在降低新型生物医学体心立方（BCC） Nb30Ti30Zr30Cr5Mo5 MEA中的杨氏模量的潜力。在高温单轴压缩下，在压缩平面上制备{001}取向晶粒是由所谓的优先动态晶粒生长控制的。在1073 ~ 1473 K的温度下，以1 × 10−4 ~ 1 × 10−2 s−1至−1.0的真应变速率进行单轴压缩。1473 K压缩后的显微组织以动态再结晶为主。真实应变速率的降低促进了{001}取向晶粒的形成，这是由于晶粒优先动态生长的增强。在1473 K、应变速率为5.0 × 10−4 s−1的压缩条件下，观察到{001}织构的最大体积分数（~ 64%）。{001}织构体积分数的增加降低了杨氏模量。与高温变形前初始样品的~ 93 GPa相比，本研究中的杨氏模量可降低至68 GPa。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

求助全文

约1分钟内获得全文求助全文

来源期刊

Intermetallics 工程技术-材料科学：综合

CiteScore

7.80

自引率

9.10%

发文量

291

审稿时长

37 days

期刊介绍： This journal is a platform for publishing innovative research and overviews for advancing our understanding of the structure, property, and functionality of complex metallic alloys, including intermetallics, metallic glasses, and high entropy alloys. The journal reports the science and engineering of metallic materials in the following aspects: Theories and experiments which address the relationship between property and structure in all length scales. Physical modeling and numerical simulations which provide a comprehensive understanding of experimental observations. Stimulated methodologies to characterize the structure and chemistry of materials that correlate the properties. Technological applications resulting from the understanding of property-structure relationship in materials. Novel and cutting-edge results warranting rapid communication. The journal also publishes special issues on selected topics and overviews by invitation only.