Crystal Structure Analysis of 1, 4, 7-Trithia-10, 13-diazacyclopentadecane-9, 14-dione

IF 0.6 4区化学 Q4 CRYSTALLOGRAPHY

Journal of Chemical Crystallography Pub Date : 2025-06-12 DOI:10.1007/s10870-025-01054-5

Timothy M.E. Jugovic, Christopher G. Hamaker

引用次数: 0

Abstract

The compound 1,4,7-trithia-10,13-diazacyclopentadecane-9,14-dione, 1, crystallizes in the space group P2₁/c with a = 9.3608(3) Å, b = 16.0333(5) Å, c = 9.5608(3) Å, β = 113.3521(14)°, and Z = 4. The title molecule forms chains via face-to-face N–H^…O hydrogen bonds. The structure of 1 is also compared to the previously reported oxygen analog, 1,4,7-trioxa-10,13-diazacyclopentadecane-9,14-dione.

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1,4,7 - trithia - 10,13 -重氮环戊烷- 9,14 -二酮的晶体结构分析

化合物1,4,7-trithia-10,13-diazacyclopentadecane-9,14-dione， 1在P21/c空间群中结晶，a = 9.3608(3) Å， b = 16.0333(5) Å， c = 9.5608(3) Å， β = 113.3521（14）°，Z = 4。标题分子通过面对面的N-H…O氢键形成链。1的结构也与先前报道的氧类似物1,4,7-三氧-10,13-二氮环戊烷-9,14-二酮进行了比较。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

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来源期刊

Journal of Chemical Crystallography 化学-光谱学

CiteScore

1.50

自引率

12.50%

发文量

审稿时长

6.3 months

期刊介绍： Journal of Chemical Crystallography is an international and interdisciplinary publication dedicated to the rapid dissemination of research results in the general areas of crystallography and spectroscopy. Timely research reports detail topics in crystal chemistry and physics and their relation to problems of molecular structure; structural studies of solids, liquids, gases, and solutions involving spectroscopic, spectrometric, X-ray, and electron and neutron diffraction; and theoretical studies.