The Thermal Expansion of Lanthanum Zirconate Ceramics

IF 0.3 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY
V. R. Khrustov, A. S. Kaygorodov, S. V. Zayats
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引用次数: 0

Abstract

The high-temperature behavior of lanthanum zirconate ceramics was studied depending on the conditions of La2Zr2O7 synthesis and sintering. Lanthanum zirconate was obtained by solid-phase synthesis, the ceramics were sintered in the temperature range of 1500–1550°C at different holding times. Thermal expansion and shrinkage activity of ceramics were studied by dilatometric analysis. Linear thermal expansion coefficients (LTECs) were determined in the temperature range of 200–1200°C during heating and cooling. The LTEC of the obtained ceramics is 9.1 × 10–6 1/K, which is significantly less than the LTEC of tetragonal zirconium dioxide doped with yttria (YSZ), 13.5 × 10–6 1/K. The LTEC decreases as the density of the ceramics increases. The microhardness of synthesized ceramics is 6.3 GPa.

Abstract Image

锆酸镧陶瓷的热膨胀
根据La2Zr2O7的合成和烧结条件,研究了锆酸镧陶瓷的高温行为。采用固相合成法制备锆酸镧,在1500 ~ 1550℃的温度范围内进行不同保温时间的烧结。用膨胀分析方法研究了陶瓷的热膨胀和收缩活性。在加热和冷却的200-1200℃范围内测定了线性热膨胀系数(LTECs)。所得陶瓷的LTEC为9.1 × 10-6 1/K,明显小于掺钇的四方二氧化锆(YSZ)的13.5 × 10-6 1/K。LTEC随陶瓷密度的增加而降低。合成陶瓷的显微硬度为6.3 GPa。
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来源期刊
Inorganic Materials: Applied Research
Inorganic Materials: Applied Research Engineering-Engineering (all)
CiteScore
0.90
自引率
0.00%
发文量
199
期刊介绍: Inorganic Materials: Applied Research  contains translations of research articles devoted to applied aspects of inorganic materials. Best articles are selected from four Russian periodicals: Materialovedenie, Perspektivnye Materialy, Fizika i Khimiya Obrabotki Materialov, and Voprosy Materialovedeniya  and translated into English. The journal reports recent achievements in materials science: physical and chemical bases of materials science; effects of synergism in composite materials; computer simulations; creation of new materials (including carbon-based materials and ceramics, semiconductors, superconductors, composite materials, polymers, materials for nuclear engineering, materials for aircraft and space engineering, materials for quantum electronics, materials for electronics and optoelectronics, materials for nuclear and thermonuclear power engineering, radiation-hardened materials, materials for use in medicine, etc.); analytical techniques; structure–property relationships; nanostructures and nanotechnologies; advanced technologies; use of hydrogen in structural materials; and economic and environmental issues. The journal also considers engineering issues of materials processing with plasma, high-gradient crystallization, laser technology, and ultrasonic technology. Currently the journal does not accept direct submissions, but submissions to one of the source journals is possible.
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