{"title":"Experimental investigation on anelasticity-controlled cyclic creep behavior in multiscale hybrid-reinforced TiAl alloys","authors":"Zhenquan Liang , Shulong Xiao , Qingchao Li , Lijuan Xu , Xiang Xue , Jing Tian , Yuyong Chen , Hao Wang","doi":"10.1016/j.ijfatigue.2025.109244","DOIUrl":null,"url":null,"abstract":"<div><div>As hot-end components in aero-engines, TiAl alloys are expected to experience cyclic creep in service. In this work, hybrid-reinforced TiAl alloys with superior creep resistance were developed through synergistic micro-alloying of C and Y<sub>2</sub>O<sub>3</sub> combined with long-term annealing. Monotonic and cyclic creep tests under various loading conditions were conducted to specifically investigate the cyclic creep behavior of the hybrid-reinforced TiAl alloys. The results indicate that, compared with monotonic creep, cyclic creep exhibits a longer rupture life and a lower strain rate due to anelastic recovery. However, the introduction of cyclic loading enhances the intrinsic creep deformation capacity of TiAl alloys due to primary creep regeneration effect, and accelerates the intrinsic creep damage, resulting in a shorter creep endurance life. Two dominant anelastic recovery mechanisms associated with dislocation cells and dislocation pile-ups were revealed. Moreover, the presence of hybrid reinforcements enhances the anelastic recovery extent. The effects of various loading parameters, including the peak stress dwell time, stress ratio, and temperature, on the macroscopic cyclic creep response were clarified. The microscopic cyclic creep deformation and failure mechanisms, as well as the dynamic precipitation behavior of Ti<sub>2</sub>AlC within the B2 phase were elucidated. A comprehensive understanding of cyclic creep behavior from both macroscopic and microscopic perspectives will help advance the structural integrity assessment of TiAl alloys.</div></div>","PeriodicalId":14112,"journal":{"name":"International Journal of Fatigue","volume":"202 ","pages":"Article 109244"},"PeriodicalIF":6.8000,"publicationDate":"2025-08-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Fatigue","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0142112325004414","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"ENGINEERING, MECHANICAL","Score":null,"Total":0}
引用次数: 0
Abstract
As hot-end components in aero-engines, TiAl alloys are expected to experience cyclic creep in service. In this work, hybrid-reinforced TiAl alloys with superior creep resistance were developed through synergistic micro-alloying of C and Y2O3 combined with long-term annealing. Monotonic and cyclic creep tests under various loading conditions were conducted to specifically investigate the cyclic creep behavior of the hybrid-reinforced TiAl alloys. The results indicate that, compared with monotonic creep, cyclic creep exhibits a longer rupture life and a lower strain rate due to anelastic recovery. However, the introduction of cyclic loading enhances the intrinsic creep deformation capacity of TiAl alloys due to primary creep regeneration effect, and accelerates the intrinsic creep damage, resulting in a shorter creep endurance life. Two dominant anelastic recovery mechanisms associated with dislocation cells and dislocation pile-ups were revealed. Moreover, the presence of hybrid reinforcements enhances the anelastic recovery extent. The effects of various loading parameters, including the peak stress dwell time, stress ratio, and temperature, on the macroscopic cyclic creep response were clarified. The microscopic cyclic creep deformation and failure mechanisms, as well as the dynamic precipitation behavior of Ti2AlC within the B2 phase were elucidated. A comprehensive understanding of cyclic creep behavior from both macroscopic and microscopic perspectives will help advance the structural integrity assessment of TiAl alloys.
期刊介绍:
Typical subjects discussed in International Journal of Fatigue address:
Novel fatigue testing and characterization methods (new kinds of fatigue tests, critical evaluation of existing methods, in situ measurement of fatigue degradation, non-contact field measurements)
Multiaxial fatigue and complex loading effects of materials and structures, exploring state-of-the-art concepts in degradation under cyclic loading
Fatigue in the very high cycle regime, including failure mode transitions from surface to subsurface, effects of surface treatment, processing, and loading conditions
Modeling (including degradation processes and related driving forces, multiscale/multi-resolution methods, computational hierarchical and concurrent methods for coupled component and material responses, novel methods for notch root analysis, fracture mechanics, damage mechanics, crack growth kinetics, life prediction and durability, and prediction of stochastic fatigue behavior reflecting microstructure and service conditions)
Models for early stages of fatigue crack formation and growth that explicitly consider microstructure and relevant materials science aspects
Understanding the influence or manufacturing and processing route on fatigue degradation, and embedding this understanding in more predictive schemes for mitigation and design against fatigue
Prognosis and damage state awareness (including sensors, monitoring, methodology, interactive control, accelerated methods, data interpretation)
Applications of technologies associated with fatigue and their implications for structural integrity and reliability. This includes issues related to design, operation and maintenance, i.e., life cycle engineering
Smart materials and structures that can sense and mitigate fatigue degradation
Fatigue of devices and structures at small scales, including effects of process route and surfaces/interfaces.