Direct laser writing for rapid fabrication of porous carbon: Enhancing Si-C reaction bonding in silicon carbide ceramics

IF 6.2 2区 材料科学 Q1 MATERIALS SCIENCE, CERAMICS
Changcong Huang , Jian Chen , Shengjun Liao , Chenxi Gao , Lan Peng , Zhongming Chen , Xuejian Liu , Zhengren Huang
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引用次数: 0

Abstract

Reaction bonding is a preferred method for joining silicon carbide ceramics, with the formation of a porous carbon reaction layer being critical for effective Si–C bonding. In this study, a porous carbon layer was rapidly fabricated using direct laser writing and applied in the reaction bonding of silicon carbide ceramics. Optimization of laser parameters and joining temperature produced a well-defined porous reaction layer, which improved the proportion and distribution of silicon carbide in the joining layer, thereby enhancing joint strength. At a laser power of 30 W and a joining temperature of 1600 °C, the joint achieved a flexure strength of 233 ± 16 MPa. Subsequent annealing and oxidation treatments increased the strength to 306 ± 23 MPa. The bonded components also exhibited excellent high-temperature performance, maintaining a strength of 214 ± 16 MPa at 1300 °C.
快速制备多孔碳的直接激光写入:增强碳化硅陶瓷中的硅-碳反应键合
反应键合是连接碳化硅陶瓷的首选方法,多孔碳反应层的形成对于有效的Si-C键合至关重要。本研究采用激光直接写入技术快速制备多孔碳层,并将其应用于碳化硅陶瓷的反应键合。通过对激光参数和连接温度的优化,形成了定义良好的多孔反应层,改善了碳化硅在连接层中的比例和分布,从而提高了连接强度。当激光功率为30 W,焊接温度为1600℃时,接头的抗折强度为233 ± 16 MPa。随后的退火和氧化处理将强度提高到306 ± 23 MPa。在1300℃时,复合材料的强度可达214 ± 16 MPa。
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来源期刊
Journal of The European Ceramic Society
Journal of The European Ceramic Society 工程技术-材料科学:硅酸盐
CiteScore
10.70
自引率
12.30%
发文量
863
审稿时长
35 days
期刊介绍: The Journal of the European Ceramic Society publishes the results of original research and reviews relating to ceramic materials. Papers of either an experimental or theoretical character will be welcomed on a fully international basis. The emphasis is on novel generic science concerning the relationships between processing, microstructure and properties of polycrystalline ceramics consolidated at high temperature. Papers may relate to any of the conventional categories of ceramic: structural, functional, traditional or composite. The central objective is to sustain a high standard of research quality by means of appropriate reviewing procedures.
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