Mohammad H. Ati , Basil A. Saleh , Adnan J. M. Al-Fartosy , Gamal A. El-Hiti , Benson M. Kariuki
{"title":"2-{(E)-[(2-Hydroxy-1-phenylethyl)imino]methyl}-4-[(E)-(4-methylphenyl)diazenyl]phenol","authors":"Mohammad H. Ati , Basil A. Saleh , Adnan J. M. Al-Fartosy , Gamal A. El-Hiti , Benson M. Kariuki","doi":"10.1107/S2414314625005991","DOIUrl":null,"url":null,"abstract":"<div><div>Intramolecular O1—H1⋯N3 hydrogen bonding occurs in the title molecule and intermolecular O—H⋯O hydrogen bonds form chains parallel to the <em>b</em> axis.</div></div><div><div>In the title compound, C<sub>22</sub>H<sub>21</sub>N<sub>3</sub>O<sub>2</sub>, an intramolecular O—H⋯N hydrogen bond is observed between the phenol and methanimine groups of the molecule. The 2-phenylethan-1-ol part is disordered over two orientations [occupancies 0.566 (17) and 0.434 (17)]. In the crystal, disordered intermolecular O—H⋯O hydrogen bonds between adjacent molecules form chains parallel to the <em>b</em> axis.<blockquote><div><span><figure><span><img><ol><li><span><span>Download: <span>Download high-res image (225KB)</span></span></span></li><li><span><span>Download: <span>Download full-size image</span></span></span></li></ol></span></figure></span></div></blockquote></div></div>","PeriodicalId":94324,"journal":{"name":"IUCrData","volume":"10 7","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2025-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"IUCrData","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S2414314625000707","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
Intramolecular O1—H1⋯N3 hydrogen bonding occurs in the title molecule and intermolecular O—H⋯O hydrogen bonds form chains parallel to the b axis.
In the title compound, C22H21N3O2, an intramolecular O—H⋯N hydrogen bond is observed between the phenol and methanimine groups of the molecule. The 2-phenylethan-1-ol part is disordered over two orientations [occupancies 0.566 (17) and 0.434 (17)]. In the crystal, disordered intermolecular O—H⋯O hydrogen bonds between adjacent molecules form chains parallel to the b axis.
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