Carren Nyapola , Sizwe J. Zamisa , Bernard Omondi , Eric M. Njogu
{"title":"5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate","authors":"Carren Nyapola , Sizwe J. Zamisa , Bernard Omondi , Eric M. Njogu","doi":"10.1107/S2414314625003372","DOIUrl":null,"url":null,"abstract":"<div><div>A two-dimensional supramolecular architecture mediated by N—H⋯N and N—H⋯O hydrogen bonds is formed in the crystal of the title compound.</div></div><div><div>The title compound, 2C<sub>15</sub>H<sub>13</sub>FN<sub>2</sub>O<sub>2</sub>·CH<sub>2</sub>Cl<sub>2</sub>, crystallizes with two main molecules in the asymmetric unit with a disordered dichloromethane solvent molecule. The dihedral angles between the fluoro phenyl ring and 4<em>H</em>-pyran ring are 74.36 (15) and 80.69 (15)° in the two molecules. In the crystal, N—H⋯N and N—H⋯O hydrogen bonds link the molecules into a two-dimensional supramolecular network propagating in the (100) plane.<span><figure><span><img><ol><li><span><span>Download: <span>Download high-res image (310KB)</span></span></span></li><li><span><span>Download: <span>Download full-size image</span></span></span></li></ol></span></figure></span></div></div>","PeriodicalId":94324,"journal":{"name":"IUCrData","volume":"10 4","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2025-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"IUCrData","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/org/science/article/pii/S2414314625000240","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
A two-dimensional supramolecular architecture mediated by N—H⋯N and N—H⋯O hydrogen bonds is formed in the crystal of the title compound.
The title compound, 2C15H13FN2O2·CH2Cl2, crystallizes with two main molecules in the asymmetric unit with a disordered dichloromethane solvent molecule. The dihedral angles between the fluoro phenyl ring and 4H-pyran ring are 74.36 (15) and 80.69 (15)° in the two molecules. In the crystal, N—H⋯N and N—H⋯O hydrogen bonds link the molecules into a two-dimensional supramolecular network propagating in the (100) plane.
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