Laser-beam powder bed fusion and post-build annealing of polycrystalline Fe81Ga19 alloys: Microstructure manipulation and magnetostrictive properties

IF 4.3 2区 材料科学 Q2 CHEMISTRY, PHYSICAL
Chengde Gao , Xiong Yao , Qi Zeng , Wei Tan , Shuaishuai Zhu , Ping Wu , Cijun Shuai
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Abstract

Magnetostrictive polycrystalline Fe-Ga alloys are gaining increasing attention for boarder practicalities, unfortunately, always facing limitations in magnetostrictive properties hindered by random grain structure and complex phase composition. In this work, an innovative method was established to fabricate massive polycrystalline Fe81Ga19 alloys via laser-beam powder bed fusion (LPBF) followed by post-build annealing treatment, and the magnetostrictive performances of the LPBF-fabricated Fe-Ga alloys annealed at various temperatures (800, 1000, and 1200 °C) were systematically investigated. Microstructural analyses revealed that <001> grain orientation and disordered A2 structure were obtained within the LPBF-fabricated (LPBFed) Fe81Ga19 alloys as a result of the steep temperature gradient and rapid solidification. Furthermore, the post-LPBF annealing treatment promoted the grain growth and release of residual stresses, simultaneously accompanied by intensified oriented texture within the annealed alloys. As a result, the Fe81Ga19 alloy annealed at 1200 °C showed optimal magnetostrictive performances with a magnetostrictive strain of ∼70 ppm and especially a 64 % reduction in saturation field relative to the LPBFed alloy. Moreover, the prepared Fe-Ga alloys also manifested good magnetostrictive dynamic response and desirable soft magnetic properties. In addition, electrochemical tests also indicated accelerated corrosion for the annealed alloys owing to the increased grain sizes. This work may pave a processing base to fabricate structure-tailored polycrystalline magnetostrictive Fe-Ga alloys for diverse applications.

Abstract Image

多晶Fe81Ga19合金的激光粉末床熔合和后期退火:显微组织操纵和磁致伸缩性能
磁致伸缩多晶Fe-Ga合金因其广泛的应用而受到越来越多的关注,但由于晶粒结构的随机性和相组成的复杂性,其磁致伸缩性能一直受到限制。本文建立了一种采用激光粉末床熔合(LPBF)制备Fe81Ga19多晶合金的新方法,并对LPBF制备的Fe-Ga合金在800、1000和1200℃不同温度下的磁致伸缩性能进行了系统研究。显微组织分析显示<001;由于温度梯度大、凝固速度快,lpbf制备的Fe81Ga19合金中出现了晶粒取向和无序A2组织。此外,后lpbf退火处理促进了晶粒的生长和残余应力的释放,同时退火合金内部的取向织构增强。结果表明,在1200℃退火的Fe81Ga19合金表现出最佳的磁致伸缩性能,磁致伸缩应变为~ 70 ppm,特别是饱和场比LPBFed合金降低了64%。此外,制备的Fe-Ga合金还表现出良好的磁致伸缩动态响应和良好的软磁性能。此外,电化学测试还表明,由于晶粒尺寸的增加,退火合金的腐蚀加速。这项工作为制造结构定制的多晶磁致伸缩Fe-Ga合金奠定了基础。
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来源期刊
Intermetallics
Intermetallics 工程技术-材料科学:综合
CiteScore
7.80
自引率
9.10%
发文量
291
审稿时长
37 days
期刊介绍: This journal is a platform for publishing innovative research and overviews for advancing our understanding of the structure, property, and functionality of complex metallic alloys, including intermetallics, metallic glasses, and high entropy alloys. The journal reports the science and engineering of metallic materials in the following aspects: Theories and experiments which address the relationship between property and structure in all length scales. Physical modeling and numerical simulations which provide a comprehensive understanding of experimental observations. Stimulated methodologies to characterize the structure and chemistry of materials that correlate the properties. Technological applications resulting from the understanding of property-structure relationship in materials. Novel and cutting-edge results warranting rapid communication. The journal also publishes special issues on selected topics and overviews by invitation only.
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