{"title":"In-situ TEM observation of <c>-axis extension twin formation at grain boundaries","authors":"Hidetoshi Somekawa , Yuka Hara , Taku Moronaga , Alok Singh , Takahito Ohmura","doi":"10.1016/j.scriptamat.2025.116575","DOIUrl":null,"url":null,"abstract":"<div><div>Effect of grain boundaries on {<span><math><mrow><mn>10</mn><mover><mn>1</mn><mo>¯</mo></mover><mn>2</mn></mrow></math></span>} twin formation and its mechanical response in Mg is investigated through in-situ TEM compression test. Compression direction is set to be normal to the <<em>c</em>>-axis, which is a favorable orientation to form {<span><math><mrow><mn>10</mn><mover><mn>1</mn><mo>¯</mo></mover><mn>2</mn></mrow></math></span>} twins. In case of a single crystal, <span><math><mrow><mo>{</mo><mn>10</mn><mover><mrow><mn>1</mn></mrow><mo>‾</mo></mover><mn>2</mn><mo>}</mo></mrow></math></span> twins form in the vicinity of the contact region of compression-tip with the specimen, as reported in previous studies. On the contrary, when the specimen has a grain boundary, this interfacial defect becomes the nucleation/formation site for twins. Stress required to form the twins is lower than that in a single crystal. Grain boundaries, which have a role in prevention of dislocation slips, create high stress fields; as a result, they lead to nucleation of a twin embryo. While twin nucleation is a probabilistic event, stress required to form the twins shows size effect.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"260 ","pages":"Article 116575"},"PeriodicalIF":5.3000,"publicationDate":"2025-01-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Scripta Materialia","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1359646225000399","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
Effect of grain boundaries on {} twin formation and its mechanical response in Mg is investigated through in-situ TEM compression test. Compression direction is set to be normal to the <c>-axis, which is a favorable orientation to form {} twins. In case of a single crystal, twins form in the vicinity of the contact region of compression-tip with the specimen, as reported in previous studies. On the contrary, when the specimen has a grain boundary, this interfacial defect becomes the nucleation/formation site for twins. Stress required to form the twins is lower than that in a single crystal. Grain boundaries, which have a role in prevention of dislocation slips, create high stress fields; as a result, they lead to nucleation of a twin embryo. While twin nucleation is a probabilistic event, stress required to form the twins shows size effect.
期刊介绍:
Scripta Materialia is a LETTERS journal of Acta Materialia, providing a forum for the rapid publication of short communications on the relationship between the structure and the properties of inorganic materials. The emphasis is on originality rather than incremental research. Short reports on the development of materials with novel or substantially improved properties are also welcomed. Emphasis is on either the functional or mechanical behavior of metals, ceramics and semiconductors at all length scales.