Obtaining and Rheological Properties of Pectin Isolated Using Microwave Radiation

IF 1.1 4区 化学 Q4 BIOCHEMISTRY & MOLECULAR BIOLOGY
L. B. Azimova, A. V. Filatova, M. Yu. Mukhamedzhanova, A. S. Turaev
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Abstract

Objective: А method has been developed for extracting modified pectin from plant raw materials by using microwave radiation at the stage of washing. Methods: The rheological properties of 5.0% aqueous solutions of apple pectin obtained by exposure to microwave radiation of various powers: 300, 450 and 600 W, as well as pectins obtained by the traditional method at temperatures of 25, 40, 55, 70°C were investigated. Results and Discussion: It is shown that the use of microwave radiation can improve the method of obtaining pectins by increasing the yield of pectins and regulating their structure and properties. The rheological properties of concentrated aqueous solutions of pectins obtained by exposure to microwave radiation of various powers have been studied. It is shown that all studied systems of pectin solutions are non-Newtonian fluids with a pseudoplastic type of viscous flow anomaly, determined by the values of the microwave energy. The values of the apparent activation energies of the viscous flow of solutions, which are an indirect characteristic of the strength of the structures of the system, have been estimated. Data was obtained on the structure and changes in the structure of their concentrated solutions under the action of external forces and temperature in the course of a viscous flow. Conclusions: It is shown that the power values оf microwave radiation are the main factor determining the structure of molecular matrices of pectins and the structure of their concentrated aqueous solutions.

Abstract Image

微波分离果胶的制备及其流变性能研究
目的:建立了在洗涤阶段利用微波辐射提取植物原料中改性果胶的方法А。方法:研究了300、450、600 W微波辐照和25、40、55、70℃微波辐照下苹果果胶5.0%水溶液的流变性能。结果与讨论:利用微波辐射可以提高果胶的收率,调节果胶的结构和性质,从而改进果胶的制备方法。研究了在不同功率微波辐射下得到的果胶浓缩水溶液的流变性能。结果表明,所研究的所有果胶溶液体系都是非牛顿流体,具有由微波能量值决定的伪塑性型粘性流动异常。溶液的黏性流动的表观活化能是体系结构强度的一个间接特征,我们估计了它的值。在粘性流动过程中,得到了它们的浓溶液在外力和温度作用下的结构和结构变化的数据。结论:微波辐射功率值是决定果胶分子基质结构及其浓水溶液结构的主要因素。
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来源期刊
Russian Journal of Bioorganic Chemistry
Russian Journal of Bioorganic Chemistry 生物-生化与分子生物学
CiteScore
1.80
自引率
10.00%
发文量
118
审稿时长
3 months
期刊介绍: Russian Journal of Bioorganic Chemistry publishes reviews and original experimental and theoretical studies on the structure, function, structure–activity relationships, and synthesis of biopolymers, such as proteins, nucleic acids, polysaccharides, mixed biopolymers, and their complexes, and low-molecular-weight biologically active compounds (peptides, sugars, lipids, antibiotics, etc.). The journal also covers selected aspects of neuro- and immunochemistry, biotechnology, and ecology.
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