{"title":"Improving parent-austenite twinned grain reconstruction using electron backscatter diffraction in low carbon austenite","authors":"Ruth M. Birch, T. Ben Britton, Warren J. Poole","doi":"10.1016/j.scriptamat.2024.116459","DOIUrl":null,"url":null,"abstract":"<div><div>Thermomechanical controlled processing (TMCP) is widely used to optimize the final properties of high strength low alloy (HSLA) steels, via microstructure engineering. The room temperature microstructures are influenced by the high temperature austenite phase, and the austenite microstructure can be accessed by reconstruction using electron backscatter diffraction (EBSD) data of the final microstructure. A challenge for reconstruction of the parent austenite grain (PAG) microstructure and subsequent austenite grain size measurement is the presence of austenite-phase annealing twins, and we address this challenge with a new ‘re-sort’ algorithm. Our algorithm has been validated using the retained austenite regions (which were recovered via advanced pattern matching of EBSD patterns). We demonstrate that the re-sort algorithm improves the PAG reconstruction significantly, especially for the grain boundary network and correlation with other methods of grain size assessment and development of TMCP steels.</div></div>","PeriodicalId":423,"journal":{"name":"Scripta Materialia","volume":"257 ","pages":"Article 116459"},"PeriodicalIF":5.3000,"publicationDate":"2024-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Scripta Materialia","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1359646224004949","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 0
Abstract
Thermomechanical controlled processing (TMCP) is widely used to optimize the final properties of high strength low alloy (HSLA) steels, via microstructure engineering. The room temperature microstructures are influenced by the high temperature austenite phase, and the austenite microstructure can be accessed by reconstruction using electron backscatter diffraction (EBSD) data of the final microstructure. A challenge for reconstruction of the parent austenite grain (PAG) microstructure and subsequent austenite grain size measurement is the presence of austenite-phase annealing twins, and we address this challenge with a new ‘re-sort’ algorithm. Our algorithm has been validated using the retained austenite regions (which were recovered via advanced pattern matching of EBSD patterns). We demonstrate that the re-sort algorithm improves the PAG reconstruction significantly, especially for the grain boundary network and correlation with other methods of grain size assessment and development of TMCP steels.
期刊介绍:
Scripta Materialia is a LETTERS journal of Acta Materialia, providing a forum for the rapid publication of short communications on the relationship between the structure and the properties of inorganic materials. The emphasis is on originality rather than incremental research. Short reports on the development of materials with novel or substantially improved properties are also welcomed. Emphasis is on either the functional or mechanical behavior of metals, ceramics and semiconductors at all length scales.