Reaction of 1-Antipyryl-4-aroyl-5-methoxycarbonyl-1H-pyrrole-2,3-diones with Ethylenediamine

IF 0.8 4区化学 Q4 CHEMISTRY, ORGANIC

Russian Journal of Organic Chemistry Pub Date : 2024-11-07 DOI:10.1134/S1070428024090276

V. A. Lyadov, N. V. Shavrina, E. S. Denislamova, A. N. Maslivets

引用次数: 0

Abstract

Methyl 3-aroyl-1-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2,4-dihydroxy-5-oxo-2,5-dihydro-1H-pyrrole-2-carboxylates reacted with ethylenediamine to give methyl-5-aryl-8-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-6,7-dioxo-2,3,4,6,7,8-hexahydropyrrolo[2,3-e][1,4]diazepine-8a(1H)-carboxylates. The product structure was confirmed by ¹H NMR and IR spectra.

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1-Antipyryl-4-aroyl-5-methoxycarbonyl-1H-pyrrole-2,3-diones 与乙二胺的反应

3-芳酰基-1-(1,5-二甲基-3-氧代-2-苯基-2,3-二氢-1H-吡唑-4-基)-2,4-二羟基-5-氧代-2,5-二氢-1H-吡咯-2-羧酸甲酯与乙二胺反应，得到甲基-5-芳酰基-8-(1、5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-6,7-dioxo-2,3,4,6,7,8-hexahydropyrrolo[2,3-e][1,4]diazepine-8a(1H)-carboxylates.1H NMR 和 IR 光谱证实了产品的结构。

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来源期刊

Russian Journal of Organic Chemistry 化学-有机化学

CiteScore

1.40

自引率

25.00%

发文量

139

审稿时长

3-6 weeks

期刊介绍： Russian Journal of Organic Chemistry is an international peer reviewed journal that covers all aspects of modern organic chemistry including organic synthesis, theoretical organic chemistry, structure and mechanism, and the application of organometallic compounds in organic synthesis.