Influence of Heat Treatment on the Microstructure and Mechanical Properties of TC4 Alloy Fabricated by Selective Laser Melting

IF 0.9 4区 材料科学 Q3 MATERIALS SCIENCE, CERAMICS
Nan Zhang, Pan Ma, Yacheng Fang, Shiguang Wan, Hong Yang
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Abstract

The TC4 (Ti6Al4V) titanium alloy fabricated by Selective Laser Melting (SLM) has gained significant attention in recent years due to its exceptional properties, including high strength-toweight ratio, excellent corrosion resistance, and biocompatibility. This study examines the effect of heat treatment on the microstructure, phase composition, and mechanical properties of SLMfabricated TC4 alloy, to provide a more comprehensive understanding of the material's behavior under varying thermal conditions. Experimental results demonstrated that the as-deposited TC4 alloy has a relative density above 0.99. The as-deposited TC4 alloy was mainly composed of closepacked hexagonal structure α/ α′ phases. In addition, a small amount of β-phase was also detected. After annealing treatment, the TC4 alloy showed a similar phase composition. The microstructure of the as-deposited TC4 alloy was composed of acicular martensite a′phase accompanied by α-phase in β-matrix. After annealing treatment, the acicular α′ martensite decomposed, transforming the microstructure into a lamellar structure consisting of α- and β-phases. The microhardness was to 351.7 HV0.2, the tensile strength was approximately 1,120 MPa, and the yield strength comprised approximately 1,080 MPa of the TC4 alloy fabricated by SLM. The tensile fracture surface of the asdeposited alloy demonstrated a mixture of brittle and ductile fracture. A quasi-cleavage river pattern and a small amount of irregular dimples can be observed. After annealing treatment, the elongation increased to 16.5% due to a slight decrease in hardness and tensile strength. The Vickers hardness was 323.1 HV0.2, the tensile strength was approximately 960 MPa, and the yield strength was about 925 MPa, respectively. The amounts and the size of dimples increased significantly and displayed typical ductile fracture. This research would provide valuable insights into optimizing the performance of SLM-fabricated TC4 alloys for various engineering applications.

Abstract Image

热处理对选择性激光熔化制造的 TC4 合金微观结构和机械性能的影响
近年来,通过选择性激光熔融(SLM)技术制造的 TC4(Ti6Al4V)钛合金因其卓越的性能,包括高强度-重量比、优异的耐腐蚀性和生物相容性而备受关注。本研究探讨了热处理对 SLM 制造的 TC4 合金的微观结构、相组成和机械性能的影响,以便更全面地了解材料在不同热条件下的行为。实验结果表明,沉积 TC4 合金的相对密度高于 0.99。沉积后的 TC4 合金主要由紧密堆积的六方结构 α/α′ 相组成。此外,还检测到少量的 β 相。退火处理后,TC4 合金显示出类似的相组成。沉积后的 TC4 合金的微观结构由锥形马氏体 a′相和β基体中的α相组成。退火处理后,针状α′马氏体分解,微观结构转变为由α相和β相组成的层状结构。通过 SLM 制造的 TC4 合金的显微硬度为 351.7 HV0.2,抗拉强度约为 1,120 兆帕,屈服强度约为 1,080 兆帕。沉积合金的拉伸断裂面显示出脆性和韧性断裂的混合。可以观察到准劈裂河纹和少量不规则凹陷。退火处理后,由于硬度和抗拉强度略有下降,伸长率增至 16.5%。维氏硬度为 323.1 HV0.2,抗拉强度约为 960 兆帕,屈服强度约为 925 兆帕。凹痕的数量和大小显著增加,并显示出典型的韧性断裂。这项研究将为优化 SLM 制造的 TC4 合金在各种工程应用中的性能提供有价值的见解。
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来源期刊
Powder Metallurgy and Metal Ceramics
Powder Metallurgy and Metal Ceramics 工程技术-材料科学:硅酸盐
CiteScore
1.90
自引率
20.00%
发文量
43
审稿时长
6-12 weeks
期刊介绍: Powder Metallurgy and Metal Ceramics covers topics of the theory, manufacturing technology, and properties of powder; technology of forming processes; the technology of sintering, heat treatment, and thermo-chemical treatment; properties of sintered materials; and testing methods.
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