Performance evaluation of high early strength micro-expansion geopolymer grout potentially used for sustainable road infrastructure

Abstract

This study aimed to develop a high early strength micro-expansion geopolymer grout material derived from recycled concrete and ground granulated blast-furnace slag (GGBS), which can be used to fill the subgrade voids and strengthen weak subgrade. A series of grout materials with varying proportions of recycled concrete were prepared, and their setting time, flowability, and strength characteristics were evaluated. The results indicated that the grout material containing 50 % recycled concrete had a final setting time of 29 min, a flow time of 15.2 s, and a 7-day compressive strength of 40.6 MPa, all of which met the requirements for subgrade grout materials. To further enhance the performance of the grout, the additives including 2 % calcium chloride (CaCl₂), 5 % magnesium oxide (MgO), and 5 % united expansive agent (UEA) were used. Results showed that the samples containing 50 % recycled concrete and 2 % CaCl₂ exhibited a 26.5 % increase in strength after 100 min of curing, while MgO and UEA reduced shrinkage by 112.5 % and 90.0 %, respectively. Additionally, microstructural analysis using SEM and XRD provided valuable insights into the complex interactions between components and their effects on material integrity. The results demonstrated that the use of CaCl₂ accelerated the hydration reaction, enhancing early strength, while the expansion agents MgO and UEA mitigated shrinkage and achieved micro-expansion at low concrete content. This study addresses environmental concerns by incorporating recycled materials, positioning the developed geopolymer grout as a sustainable, high-performance alternative in road construction. Integrating waste-derived components and innovative additives represents a significant step towards advancing sustainable practices in infrastructure development.