Effect of aging treatment on the microstructure, cracking type and crystallographic texture of IN939 fabricated by powder bed fusion-laser beam

Abstract

This study aimed to provide a comprehensive understanding of how aging treatments (namely, HT1 and HT2) affect the microstructure, cracking behavior, and crystallographic texture of IN939 fabricated by powder bed fusion-laser beam (PBF-LB) method. Although both aged samples demonstrated similar grain structure and recrystallization behavior according to the electron backscatter diffraction (EBSD) analysis, as well as the precipitation of bimodal γ′ phase and MC- and M₂₃C₆-type carbides, notable differences were observed in the size and morphology, particularly the γ′ phase. The HT1 sample displayed coarsened primary γ′ phase, with sizes reaching up to 2 μm and exhibiting varied morphologies, including irregular and cuboidal shapes. Additionally, this treatment led to the formation of some γ′-γ eutectic regions and plate-like η phase, along with the decomposition of MC-type carbides into M₂₃C₆-type carbides. In contrast, the HT2 sample displayed uniformly distributed spherical primary γ′ phase with sizes ranging from 70 to 120 nm, accompanied by very fine secondary γ′ phase. Furthermore, it was found that changes in both aged sample microstructures could result in the formation of strain-age cracks due to the γ′ phase formation and liquation cracks due to the partial remelting of lower melting point phases. The findings also revealed that with the application of aging treatments, the hardness of the as-fabricated sample (339.8 ± 3.4 HV) increased to 440.2 ± 5.6 HV and 508.1 ± 4.8 HV for the heat treatment of HT1 and HT2, respectively.