Macro and Nano Experimental Facts Verifying the Colloidal Process in Silver Mirror Reaction

IF 2.9 3区 教育学 Q2 CHEMISTRY, MULTIDISCIPLINARY
Yiping Wang, Jun Cao*, Jiaxin Zhang, Xilian Cao, Hong Yao and Ronghui Que*, 
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引用次数: 0

Abstract

This lab activity explored the overlooked process of the silver mirror reaction by conducting experiments at both macro and nano scale. At the macro scale, laser irradiation on a reaction container revealed a gradually noticeable Tyndall effect. At the nano scale, silver nanoparticles (AgNPs) were collected at different periods during the reaction and characterized using UV–vis spectrometer and transmission electron microscopy (TEM). The UV–vis spectra exhibited a red-shift trend between characteristic wavelengths of AgNPs, and an increase in the absorption peak as time progressed. Additionally, TEM images and particle sizes revealed a gradual increase in the average diameter of AgNPs. These experimental facts verify the colloidal process in the silver mirror reaction. This lab activity was carried out by a group of students majoring in chemistry at Anhui Normal University. Satisfactory teaching effects have been achieved.

Abstract Image

验证银镜反应胶体过程的宏观和纳米实验事实
本实验活动通过在宏观和纳米尺度上进行实验,探索了银镜反应的俯视过程。在宏观尺度上,激光照射反应容器会发现逐渐明显的廷德尔效应。在纳米尺度上,在反应的不同时期收集银纳米粒子(AgNPs),并使用紫外可见光谱仪和透射电子显微镜(TEM)对其进行表征。紫外-可见光谱显示了 AgNPs 特征波长之间的红移趋势,并且随着时间的推移,吸收峰值也在增加。此外,TEM 图像和粒度显示 AgNPs 的平均直径逐渐增大。这些实验事实验证了银镜反应中的胶体过程。该实验活动由安徽师范大学化学专业的一组学生进行。取得了令人满意的教学效果。
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来源期刊
Journal of Chemical Education
Journal of Chemical Education 化学-化学综合
CiteScore
5.60
自引率
50.00%
发文量
465
审稿时长
6.5 months
期刊介绍: The Journal of Chemical Education is the official journal of the Division of Chemical Education of the American Chemical Society, co-published with the American Chemical Society Publications Division. Launched in 1924, the Journal of Chemical Education is the world’s premier chemical education journal. The Journal publishes peer-reviewed articles and related information as a resource to those in the field of chemical education and to those institutions that serve them. JCE typically addresses chemical content, activities, laboratory experiments, instructional methods, and pedagogies. The Journal serves as a means of communication among people across the world who are interested in the teaching and learning of chemistry. This includes instructors of chemistry from middle school through graduate school, professional staff who support these teaching activities, as well as some scientists in commerce, industry, and government.
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