Mechanical properties improvement of titanium alloy and its grain boundary dislocation evolution mechanism by novel electroshock treatment

Zhongmei Wang, Jue Lu, Yanli Song, Yongqing Yu, Yuhang Wu, Lechun Xie, Lin Hua
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Abstract

Titanium alloys are extensively utilized in the aerospace industry due to their exceptional strength and resistance to corrosion. However, litmited performance and high dispersion has always existed for the traditional manufacturing process. A novel Electroshock Treatment (EST) procedure proposed by author's team can synergistically improve the mechanical properties and its consistency of titanium alloys under limited temperature rise, but the relevant mechanism is not yet clear. In present work, the effects of various EST conditions on the mechanical characteristics were investigated by uniaxial tensile testing, and the effect mechanism was revealed using multi-scale microstructure characterization of titanium alloys, such as SEM, EBSD and TEM. The uniaxial tensile test results show that, compared with the sample without EST, the average elongation after fracture improved by 12.5%, the strength-plastic product improved by 16.1%, and the consistency of UTS and elongation after fracture improved by 63.4% and 57.1%, respectively, with a slight increase of tensile strength (30 MPa) after appropriate treatment (current density of 0.93 × 10A/m, and pulse duration of 300 ms). The multi-scale microscopic characterization reveals a more uniform distribution of stress concentration in TC11 titanium alloy following the appropriate EST process. Besides, the entanglement of dislocations is reduced with some dislocations being annihilated. Especially, the remaining dislocations undergoing orderly rearrangement at grain boundaries after EST. The homogenization of local lattice distortion distribution and orderly rearrangement of dislocations at grain boundaries are the primary factors contributing to the comprehensive improvement in the mechanical properties and consistency of TC11 Titanium alloy.
新型电击处理对钛合金机械性能的改善及其晶界位错演化机制
钛合金因其卓越的强度和抗腐蚀性而被广泛应用于航空航天工业。然而,传统的制造工艺一直存在性能受限和高分散性的问题。作者团队提出的一种新型电击处理(EST)程序可在有限的温升条件下协同改善钛合金的机械性能及其一致性,但相关机理尚不清楚。本研究通过单轴拉伸试验研究了各种EST条件对力学性能的影响,并利用扫描电镜、EBSD和TEM等多尺度钛合金微观结构表征揭示了其影响机理。单轴拉伸试验结果表明,与未进行EST处理的样品相比,经过适当处理(电流密度为0.93×10A/m,脉冲持续时间为300 ms)后,断裂后平均伸长率提高了12.5%,强度塑性积提高了16.1%,UTS和断裂后伸长率的一致性分别提高了63.4%和57.1%,抗拉强度(30 MPa)略有提高。多尺度微观表征显示,经过适当的EST处理后,TC11钛合金的应力集中分布更加均匀。此外,位错的缠结减少,部分位错被湮灭。特别是在EST后,剩余的位错在晶界处进行了有序的重新排列。局部晶格畸变分布的均匀化和晶界位错的有序重排是 TC11 钛合金的机械性能和一致性得到全面改善的主要因素。
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