Microstructural behavior of mortars containing thermo-activated crushed demolition residue (TCDR)

Abstract

The construction industry has been constantly expanding and is, consequently responsible for a high consumption volume of natural raw materials and for generating large amounts of waste. In detriment of this scenario, this research proposes the reuse of Construction and Demolition Waste (CDW), especially that from plaster for making mortars. The residue was thermo-activated at 650 °C for a period of 2h, a heating rate of 10 °C/min, it was crushed in a jaw crusher and passed through an ABNT N° 16 sieve. The mortars were prepared with a (cement:sand) ratio of 1:6 by mass, the sand was partially replaced by the residue in proportions of 0, 10, 20 and 30%, using Ordinary Portland Cement (OPC). Tests were carried out on consistency index, mass density, incorporated air content, isothermal calorimetry, water retention, mass density in the hardened state, flexural strength, compressive strength, water absorption and void index, in addition to testing techniques characterization, such as laser granulometry, pozzolanic activity using the Modified Chapelle method and Lúxan method, X-Ray Fluorescence (XRF), X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) as well as Mercury Intrusion Porosimetry (MIP). It was possible to observe that the residue has amorphous phases, through XRD and heterogeneous nucleation of smaller particles, proven by the calorimetry test, contributing to the increase in mechanical strength. The results indicate that the mixture with 30% replacement achieved a greater increase in mechanical strength, lower absorption rates and consequently, a reduction in the distribution of pore sizes.