Effect of applied load on wear of microwave sintered alumina-graphene ceramic composite material

K. I. V. Vandana, M. Rajyalakshmi, Sri Chaitanya Ch
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Abstract

Ceramic materials are of technical and commercial importance and can meet many engineering requirements owing to their thermal, chemical and mechanical performance. Due to its high density and hardness, alumina (Al2O3) is one of the main materials in this category that can be used to produce critical parts. An example of such an application is wear and abrasion resistance. The fabrication root technique and a suitable secondary reinforcement material can enhance a ceramic's wear characteristics. Hence the present work is mainly concentrated on the preparation of alumina ceramic composite material reinforced with different weight proportions of graphene ranging from 0.15wt% to 0.45 wt% (with an interval of 0.1) and fabrication through microwave sintering method. Wear studies are performed on graphene reinforced alumina ceramic material samples using pin-on-disk apparatus at different loads of 5N, 10N, 15N keeping speed of 0.8 m/sec and sliding distance of 40 m constant. The obtained wear results are compared with wear performance of pure alumina samples which are prepared in the same condition. Wear tests even at higher load of 15N revealed that the decrease in wear rate of the composite samples reinforced with 0.35 wt% of grapheme is 35.14% and in the composite samples reinforced with 0.45 wt% of graphene is 34.85% when compared with wear rate of monolithic alumina samples. The effect of different wt%s of graphene on wear properties of obtained ceramic composite is also studied through SEM analysis.
外加载荷对微波烧结氧化铝-石墨烯陶瓷复合材料磨损的影响
陶瓷材料具有重要的技术和商业价值,由于其热、化学和机械性能,可以满足许多工程要求。氧化铝(Al2O3)具有高密度和高硬度,是这类材料中可用于生产关键部件的主要材料之一。耐磨性就是此类应用的一个例子。制造技术和合适的辅助增强材料可以提高陶瓷的耐磨特性。因此,目前的工作主要集中在制备氧化铝陶瓷复合材料,并用不同重量比例的石墨烯进行增强,石墨烯的重量比例从 0.15 wt% 到 0.45 wt%(间隔为 0.1)不等,并通过微波烧结法进行制造。在保持 0.8 米/秒的速度和 40 米的滑动距离不变的情况下,在 5N、10N 和 15N 的不同载荷下,使用针盘装置对石墨烯增强氧化铝陶瓷材料样品进行了磨损研究。获得的磨损结果与在相同条件下制备的纯氧化铝样品的磨损性能进行了比较。磨损测试显示,与整体氧化铝样品的磨损率相比,即使在 15N 的较高载荷下,使用 0.35 wt% 的石墨烯增强的复合样品的磨损率也降低了 35.14%,使用 0.45 wt% 的石墨烯增强的复合样品的磨损率降低了 34.85%。此外,还通过 SEM 分析研究了不同重量百分比的石墨烯对陶瓷复合材料磨损性能的影响。
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