Crystal structure of poly[octakis(μ-oxido)-tris(μ-1,1′-[[1,1′-biphenyl]-4,4′-diylbis(methylene)]bis(1H-imidazole))-tetrakis(oxido)-tetra-vanadium-dimanganese(II)dihydrate], C30H29MnN6O7V2
Ling-Ling Dai, Xiao-Jie Wang, Yu-Cai Qin
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{"title":"Crystal structure of poly[octakis(μ-oxido)-tris(μ-1,1′-[[1,1′-biphenyl]-4,4′-diylbis(methylene)]bis(1H-imidazole))-tetrakis(oxido)-tetra-vanadium-dimanganese(II)dihydrate], C30H29MnN6O7V2","authors":"Ling-Ling Dai, Xiao-Jie Wang, Yu-Cai Qin","doi":"10.1515/ncrs-2024-0139","DOIUrl":null,"url":null,"abstract":"\n <jats:p>C<jats:sub>30</jats:sub>H<jats:sub>29</jats:sub>MnN<jats:sub>6</jats:sub> O<jats:sub>7</jats:sub>V<jats:sub>2</jats:sub>, triclinic, <jats:italic>P</jats:italic>\n <jats:inline-formula id=\"j_ncrs-2024-0139_ineq_001\">\n <jats:alternatives>\n <m:math xmlns:m=\"http://www.w3.org/1998/Math/MathML\" overflow=\"scroll\">\n <m:mrow>\n <m:mover accent=\"true\">\n <m:mn>1</m:mn>\n <m:mo>‾</m:mo>\n </m:mover>\n </m:mrow>\n </m:math>\n <jats:tex-math>$\\overline{1}$</jats:tex-math>\n <jats:inline-graphic xmlns:xlink=\"http://www.w3.org/1999/xlink\" xlink:href=\"graphic/j_ncrs-2024-0139_ineq_001.png\"/>\n </jats:alternatives>\n </jats:inline-formula> (no. 2), <jats:italic>a</jats:italic> = 9.0806(3) Å, <jats:italic>b</jats:italic> = 11.1937(3) Å, <jats:italic>c</jats:italic> = 16.3585(5) Å, <jats:italic>α</jats:italic> = 102.2430(10)°, <jats:italic>β</jats:italic> = 100.090(1)°, <jats:italic>γ</jats:italic> = 97.7410(10)°, <jats:italic>V</jats:italic> = 1574.09(8) Å<jats:sup>3</jats:sup>, <jats:italic>Z</jats:italic> = 2, <jats:italic>R<jats:sub>gt</jats:sub>\n </jats:italic>(<jats:italic>F</jats:italic>) = 0.0335, <jats:italic>wR<jats:sub>ref</jats:sub>\n </jats:italic>(<jats:italic>F</jats:italic>\n <jats:sup>2</jats:sup>) = 0.0886, <jats:italic>T</jats:italic> = 100 K.</jats:p>","PeriodicalId":23885,"journal":{"name":"Zeitschrift für Kristallographie - New Crystal Structures","volume":" 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2024-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Zeitschrift für Kristallographie - New Crystal Structures","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1515/ncrs-2024-0139","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
C30 H29 MnN6 O7 V2 , triclinic, P
1
‾
$\overline{1}$
(no. 2), a = 9.0806(3) Å, b = 11.1937(3) Å, c = 16.3585(5) Å, α = 102.2430(10)°, β = 100.090(1)°, γ = 97.7410(10)°, V = 1574.09(8) Å3 , Z = 2, Rgt
(F ) = 0.0335, wRref
(F
2 ) = 0.0886, T = 100 K.
聚[八(μ-氧代)-三(μ-1,1′-[[1,1′-联苯]-4,4′-二基双(亚甲基)]双(1H-咪唑))-四(氧代)-四钒-二锰(II)二水合物]，C30H29MnN6O7V2 的晶体结构
C30H29MnN6 O7V2，三菱形，P 1 ‾ $overline{1}$（no.2), a = 9.0806(3) Å, b = 11.1937(3) Å, c = 16.3585(5) Å, α = 102.2430(10)°, β = 100.090(1)°, γ = 97.7410(10)°, V = 1574.09(8) Å3, Z = 2, Rgt (F) = 0.0335, wRref (F 2) = 0.0886, T = 100 K。
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