Effect of High-Temperature Annealing on the Structure and Properties of a Composite Material Based on TiC/TiB2/Ti3SiC2

IF 0.4 4区 材料科学 Q4 MATERIALS SCIENCE, CERAMICS
A. S. Konstantinov, A. P. Chizhikov, M. S. Antipov, P. M. Bazhin, N. Yu. Khomenko
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引用次数: 0

Abstract

High-temperature annealing of a composite material based on the Ti3SiC2 MAX-phase dispersion-strengthened with TiC and TiB2 particles obtained by free SHS compression was carried out. The annealing was carried out in an oxidizing atmosphere at 900, 1100, and 1300°C for 10 h and at 1400°C for 4 h. Experimental dependences of the specific weight gain of the oxidized samples and the oxidation rate on the temperature and annealing time were plotted. The effect of annealing temperature on the phase composition, structure, and mechanical properties of the materials was established based on x-ray phase analysis, scanning electron microscope images, and energy-dispersive analysis. The proportion of the MAX-phase increased from 26 to 63 wt.% as the annealing temperature of the material increased.

Abstract Image

高温退火对基于 TiC/TiB2/Ti3SiC2 的复合材料结构和性能的影响
对一种基于 Ti3SiC2 MAX 相分散体的复合材料进行了高温退火,该复合材料通过自由 SHS 压缩获得,并用 TiC 和 TiB2 颗粒进行了强化。退火在氧化气氛中进行,温度分别为 900、1100 和 1300°C,持续 10 小时;1400°C,持续 4 小时。根据 X 射线相分析、扫描电子显微镜图像和能量色散分析,确定了退火温度对材料相组成、结构和机械性能的影响。随着材料退火温度的升高,MAX 相的比例从 26% 增加到 63%。
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来源期刊
Refractories and Industrial Ceramics
Refractories and Industrial Ceramics 工程技术-材料科学:硅酸盐
CiteScore
0.90
自引率
20.00%
发文量
38
审稿时长
6-12 weeks
期刊介绍: Refractories and Industrial Ceramics publishes peer-reviewed articles on the latest developments and discoveries in the field of refractory materials and ceramics, focusing on the practical aspects of their production and use. Topics covered include: Scientific Research; Raw Materials; Production; Equipment; Heat Engineering; Applications.
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