Optimization of process parameters of 3D printed thermoplastic elastomeric materials using statistical modeling with particular reference to mechanical properties and print quality

Pratiksha Awasthi, Arun Kumar, Pulak Mohan Pandey, Shib Shankar Banerjee
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Abstract

Additive manufacturing of thermoplastic elastomeric material (TPE) using direct ink writing (DIW) based printing technique opens new horizons for various applications. However, the most crucial process in DIW 3D printing is the optimization of printing parameters to obtain high-quality products both in terms of aesthetics and strength. In this work, statistical models were developed considering layer height, print speed, and, ink concentration to obtain the optimized print quality product from the blend of thermoplastic polyurethane (TPU)/ epichlorohydrin − ethylene oxide − allyl glycidyl ether elastomer (GECO) based TPE materials. Experiments were designed according to the central composite design (CCD) scheme and the influence of input printing parameters on shrinkage and tensile strength was analyzed. The significance of each parameter was systematically studied using the response surface method. For both responses, shrinkage, and tensile strength, printing speed was found to be the most significant parameter. Ink concentration significantly affected tensile strength with a contribution of ∼ 34%. On the other hand, the layer height, with a contribution of ∼ 22% significantly affected the shrinkage behaviour of the 3D printed sample. Finally, multi-objective optimization was performed using a genetic algorithm to identify the optimal 3D printing parameters of the developed TPE materials.

利用统计建模优化 3D 打印热塑性弹性体材料的工艺参数,特别是机械性能和打印质量
基于直接墨水写入(DIW)打印技术的热塑性弹性体(TPE)增材制造为各种应用开辟了新天地。然而,DIW 三维打印中最关键的过程是优化打印参数,以获得美观和强度兼具的高质量产品。在这项工作中,建立了考虑层高、打印速度和油墨浓度的统计模型,以便从基于热塑性聚氨酯(TPU)/环氧氯丙烷-环氧乙烷-烯丙基缩水甘油醚弹性体(GECO)的混合热塑性聚氨酯材料中获得优化的打印质量产品。实验按照中央复合设计(CCD)方案进行设计,并分析了输入印刷参数对收缩率和拉伸强度的影响。使用响应面法系统地研究了每个参数的重要性。结果发现,对于收缩率和拉伸强度这两个响应,印刷速度是最重要的参数。油墨浓度对拉伸强度的影响很大,占 34%。另一方面,层高对三维打印样品的收缩性能有明显影响,影响程度为 22%。最后,利用遗传算法进行了多目标优化,以确定所开发 TPE 材料的最佳三维打印参数。
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