Extraction Characterization of Oils Extracted from different Parts of Red and Yellow Varieties of Anacardium occidentale (Lin)

N. B. Nwosu, E. E. Okoronko, D. K. Njoku, P. O. Emole
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Abstract

The objective of this study was to extract and characterized the oils from different parts of red and yellow varieties of Anacardium occidentale after extractions using Soxhlet extractor and steam distillation techniques and characterization of the bioactive components using GC/MS analysis. Physicochemical parameters of the extracted oils were analyzed, and the bioactive compositions were also examined. The results showed that the oils extracted were within 0 and 0.5% moisture content and pH values ranged from 3.7 to 4.7.  The average relative densities of the extracted oils by Soxhlet extraction and steam distillation at temperature 25oC were 0.887 and 0.8745 g/cm3 respectively, with average saponification value of 132.45 mgKOH/g for Soxhlet extraction and 127.98 mgKOH/g for steam distillation. The iodine values of all the oils were between 35 and 19.00 mg iodine/100g; while the refractive index was between 1.7 and 1.9. The acid values were within the range of 10.00 and 13.00 mgKOH/g, and peroxide value of 1.67 and 1.20 mmol/l. The oils had low viscosity which were within 28 and 32 mpa.s. The compounds identified from the GC-MS results showed that cashew nut shell oil contained cardol, anacardic acid, cardanol, 2-methyl cardol, triacconten and β-sitosterol. The main bioactive components of the extracted oil identified from the stem bark, root bark, and leaf were alkaloids, tannins, flavonoids, coumarins, terpenoids, and saponins. This study, therefore, showed that Soxhlet extraction could be a better extraction method for extraction of oil from cashew nut shell which had higher relative density; while cashew stem bark, root bark and the leaf which had lower density were selective based on the target products.
西洋柿(林)红色和黄色品种不同部位萃取油的提取特征
本研究的目的是在使用索氏提取器和蒸汽蒸馏技术萃取西洋金合欢的红色和黄色品种不同部位的油后,对其进行提取和表征,并使用气相色谱/质谱分析法对其生物活性成分进行表征。对萃取油的理化参数进行了分析,并对生物活性成分进行了检测。结果表明,萃取油的含水量在 0% 和 0.5% 之间,pH 值在 3.7 至 4.7 之间。 在温度为 25oC 的条件下,索氏提取法和蒸汽蒸馏法提取的油的平均相对密度分别为 0.887 和 0.8745 g/cm3,索氏提取法的平均皂化值为 132.45 mgKOH/g,蒸汽蒸馏法的平均皂化值为 127.98 mgKOH/g。所有油类的碘值在 35 至 19.00 毫克碘/100 克之间,折射率在 1.7 至 1.9 之间。酸值在 10.00 至 13.00 毫克 KOH/g 之间,过氧化值在 1.67 至 1.20 毫摩尔/升之间。腰果壳油的粘度较低,在 28 和 32 mpa.s 之间。气相色谱-质谱(GC-MS)鉴定结果表明,腰果壳油中含有棉酚、无患子酸、棉酚、2-甲基棉酚、三尖杉烯和β-谷甾醇。从茎皮、根皮和叶中提取的油中鉴定出的主要生物活性成分有生物碱、单宁、黄酮类、香豆素、萜类和皂苷。因此,这项研究表明,索氏提取法是从相对密度较高的腰果壳中提取油的较好提取方法;而密度较低的腰果茎皮、根皮和叶则可根据目标产物进行选择。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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