Investigation into the Use of Thevetia Peruviana seed oil for Surfactant Flooding

Kingsley Ihekoronye, Sulaiman Ibrahim, Mohammed Adamu, Usman Hassan
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Abstract

Surfactant is a surface-active agent that aids to improve oil recovery via changing the rock properties from oil-wet to water-wet. Synthetic surfactant is mostly used chemical enhanced oil recovery method but its vulnerability to high temperature and salinity reservoir pose a challenge to its application. In this study, Thevetia Peruviana oil was used as a precursor for surfactant formulation via saponification reaction. Soxhlet extraction technique was used to extract the oil from the seeds. Physicochemical properties of the extracted oil were investigated. Characterization using Fourier transform infrared spectrometer (FTIR) and X-ray fluorescence was carried out on the formulated surfactant to determine the functional groups and elemental composition. The results of this study showed that the Thevetia Peruviana seed have percentage of oil yield (61.3%), saponification value (218.79mg/100g), acid value (28.05mg/g), free fatty acid (14.03 mg/L), iodine value (9.39mg/L), specific gravity (0.90 g/cm3) and pH (4.04). The FTIR test results on the formulated surfactant showed the presence of the hydroxyl (OH) and carboxyl (COOH) functional groups. The XRF test showed major elements such as silicon, magesium, chlorine, iron and copper. This indicate that the surfactant is anionic and have
关于使用秘鲁鼠尾草种子油进行表面活性剂浸泡的研究
表面活性剂是一种表面活性剂,通过改变岩石性质,使其从油湿变为水湿,从而提高石油采收率。合成表面活性剂主要用于化学提高石油采收率的方法,但它易受高温和盐度储层的影响,这给其应用带来了挑战。在这项研究中,通过皂化反应,将秘鲁鼠尾草油用作配制表面活性剂的前体。采用索氏提取技术从种子中提取油脂。研究了萃取油的理化性质。使用傅立叶变换红外光谱仪(FTIR)和 X 射线荧光对配制的表面活性剂进行了表征,以确定其官能团和元素组成。研究结果表明,秘鲁鼠尾草种子出油率(61.3%)、皂化值(218.79 毫克/100 克)、酸值(28.05 毫克/克)、游离脂肪酸(14.03 毫克/升)、碘值(9.39 毫克/升)、比重(0.90 克/立方厘米)和 pH 值(4.04)。配制表面活性剂的傅立叶变换红外光谱测试结果显示存在羟基(OH)和羧基(COOH)官能团。XRF 测试显示了主要元素,如硅、镁、氯、铁和铜。这表明该表面活性剂是阴离子表面活性剂,具有
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