Physical Simulation of Primary Production in Duvernay Shale – Impact of Thermal Maturity on Oil Production

Amin Alinejad, Hassan Dehghanpour
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Abstract

Most unconventional wells typically exhibit limited oil production during the primary production stage, primarily due to ultralow permeability of the rock matrix and immaturity of the organic matter. To understand the key factors responsible for this limitation and identify candidate sweet spots for drilling, we conduct physical simulations of the primary production stage in the laboratory. In this study, Duvernay shale samples undergo a single-cycle methane injection process to simulate the primary production stage. We utilize a visualization cell to explore oil-recovery mechanisms under representative reservoir conditions. We soak oil-saturated core plugs with methane at 4,150 psig and a reservoir temperature of 90°C to restore initial reservoir conditions. After equilibrium, we deplete the cell pressure at a controlled rate to simulate the primary production stage. Using two shale samples with different thermal maturity levels, our results demonstrate that methane diffuses into both cores during the soaking; however, it dissolves in oil only in the mature shale sample, resulting in a live oil with a solution gas-oil ratio of 932 standard ft3/stock tank barrel. During the primary production stage, we observe significant oil production under the solution-gas drive mechanism from the mature shale, while the immature shale exhibits negligible oil production. Natural fractures enhance gas penetration into the core, contributing to increased oil production in the primary production stage. Ultimately, the mature shale sample exhibits an oil recovery factor of 25.6% of original oil-in-place after the primary production stage, a remarkable contrast to 1.5% recovery observed in the immature shale. This difference is attributed to the immaturity of the organic matter, insufficient original oil-in-place, and absence of connected oil-wet pore network in the immature shale sample, confirmed by wettability evaluation and rock-eval pyrolysis data.
杜弗奈页岩初级生产的物理模拟--热成熟度对石油生产的影响
大多数非常规油井在初级生产阶段的石油产量通常有限,这主要是由于岩石基质的超低渗透性和有机物的不成熟造成的。为了了解造成这种限制的关键因素,并确定候选钻井甜点,我们在实验室中对初级生产阶段进行了物理模拟。在这项研究中,Duvernay 页岩样本经历了单循环甲烷注入过程,以模拟初级生产阶段。我们利用可视化单元探索代表性储层条件下的石油回收机制。我们用压力为 4,150 psig、储层温度为 90°C 的甲烷浸泡油饱和岩心塞,以恢复初始储层条件。达到平衡后,我们以可控的速度耗尽岩芯压力,以模拟初级生产阶段。我们使用两种热成熟度不同的页岩样本,结果表明甲烷在浸泡过程中扩散到两种岩心中;但是,只有成熟页岩样本中的甲烷溶解在油中,形成溶液气油比为 932 标准立方英尺/储罐桶的活油。在初级生产阶段,我们观察到成熟页岩在溶液-气体驱动机制下产生大量石油,而未成熟页岩的石油产量则微乎其微。天然裂缝增强了气体向岩心的渗透,从而提高了初级生产阶段的石油产量。最终,成熟页岩样本在初级生产阶段后的石油采收率为原始原位石油的 25.6%,与未成熟页岩 1.5% 的采收率形成鲜明对比。这种差异归因于未成熟页岩样本中的有机物不成熟、原始原位油不足以及缺乏连接的油湿孔隙网络,这一点已通过润湿性评估和岩石-评价热解数据得到证实。
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