Enhanced Microhardness and Corrosion Performance of Additively Manufactured Inconel 718 Specimens through Nanostructuring by Severe Plastic Deformation

S. M. Yusuf, Nur Hidayah Musa, N. Mazlan, Nong Gao
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Abstract

Severe plastic deformation (SPD) processes, particularly high-pressure torsion (HPT) have been increasingly applied to metallic specimens fabricated by laser powder bed fusion (L-PBF) additive manufacturing (AM) for enhancing their mechanical and functional properties through nanoscale grain refinement (≤ 100 nm). In this study. L-PBF AM-fabricated Inconel 718 (IN 718) specimens are initially subjected to 10 HPT revolutions to produce nanosized grains. Subsequently, microstructural characterisation, as well as hardness and electrochemical tests are conducted to evaluate the evolution of microstructures, hardness, and corrosion performance of the as-received and HPT-processed specimens by using various microscopy, Vickers microhardness (HV) measurements, and corrosion performance, respectively. The results reveal an average grain size of ~ 46 nm, dense dislocation networks, and nanotwins after 10 HPT processing, which contribute to the two-fold hardness increase compared to the as-received condition. Such microstructures also contributed to the overall improved corrosion performance after 10 HPT processing, as quantified by the 83% and 73% reduction in corrosion rate and pitting potential, respectively.
通过剧烈塑性变形进行纳米结构化,增强快速成型 Inconel 718 试样的显微硬度和腐蚀性能
严酷塑性变形(SPD)工艺,尤其是高压扭转(HPT)工艺,已越来越多地应用于激光粉末床熔融(L-PBF)快速成型制造(AM)工艺制作的金属试样,通过纳米级(≤ 100 nm)晶粒细化提高其机械和功能特性。在这项研究中L-PBF AM 制造的 Inconel 718 (IN 718) 试样最初要经过 10 次 HPT 旋转,以产生纳米级晶粒。随后,通过各种显微镜、维氏显微硬度(HV)测量和腐蚀性能测试,分别对原样接收试样和 HPT 加工试样的微结构表征、硬度和腐蚀性能的演变进行了评估。结果表明,经过 10 次 HPT 处理后,试样的平均晶粒大小约为 46 nm,并出现了密集的位错网络和纳米细丝,与原样相比,硬度提高了两倍。10 HPT 处理后,这种微结构还有助于全面提高腐蚀性能,腐蚀速率和点蚀电位分别降低了 83% 和 73%。
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