Green Synthesis of ZnO Nanoparticles Using Potato Extracts (Solanum tuberosum) As an Antibacterial Agent in the Active Packaging For Food Products

Supardianningsih, Susiani Susiani, M. Nugraha
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Abstract

In this work, we have implemented an eco-friendly method for synthesis of zinc oxide nanoparticles (ZnO NPs) using potato extracts (Solanum tuberosum) as the natural bio-reductants and stabilizing agent. Meanwhile the zinc nitrate octahydrate (Zn[NO3] 2.6H2O) and ammonium hydroxide (NH4OH) were used as the precursor of ZnO NPs. The sediment of Zn(OH)2 was separated from the solvent using centrifuge, and further calcinated at the temperature of 500ºC so that formed ZnO nanoparticles. SEM micrograph of ZnO NPs shows the hexagonal shapes with particles size around 50–100 nm. The XRD spectra confirms that ZnO NPs exhibited well crystalline nature, however, there were impurity peaks caused by the potato extracts addition. From the FTIR analysis, we obtained the existence of another chemical compounds, denoting the presence of stabilizing and reducing agent from potato extract. Keywords: ZnO nanoparticles, green synthesis, antibacterial and active packaging
利用马铃薯提取物(Solanum tuberosum)作为食品活性包装中的抗菌剂,绿色合成氧化锌纳米粒子
在这项工作中,我们采用了一种以马铃薯提取物(Solanum tuberosum)为天然生物还原剂和稳定剂的环保型方法来合成氧化锌纳米粒子(ZnO NPs)。同时,八水硝酸锌(Zn[NO3] 2.6H2O)和氢氧化铵(NH4OH)被用作 ZnO NPs 的前体。用离心机将 Zn(OH)2 的沉淀物从溶剂中分离出来,并在 500ºC 的温度下进一步煅烧,从而形成 ZnO 纳米粒子。ZnO NPs 的扫描电镜显微照片显示其呈六角形,颗粒大小约为 50-100 纳米。XRD 光谱证实 ZnO NPs 具有良好的结晶性,但也存在因添加马铃薯提取物而产生的杂质峰。通过傅立叶变换红外光谱分析,我们得到了另一种化合物的存在,表明马铃薯提取物中存在稳定剂和还原剂。关键词氧化锌纳米粒子 绿色合成 抗菌活性包装
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