Evaluation of magnetic and electrochemical performance of copper oxide nanoparticles using Myristica fragrans (mace) extract

Shandhiya Murugan, Deepika Balraj, Saranya Amirtharajan, Ramesh P Manimuthu, Rama R N Venkata, Janarthanan Balasundaram, Mohamed R Ziaudeen, Sharmila Saminathan
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Abstract

The synthesis of metal oxide nanoparticles using natural extract encourages the futuristic design of an environmentally friendly system by getting rid of the dangerous, toxic substances. The food industry in India is paying a lot of attention to Myristica fragrans, often known as mace, due to its rich medicinal significance. In the current study, M. fragrans (Mace) aqueous extract was used to prepare copper oxide (CuO) nanoparticles. Phytochemical screening confirms the presence of bioactive substances such as alkaloids, sterols, glycosides, and flavonoids in the extract. XRD and SEM measurements show that the nanoparticles have a monoclinic structure with polyhedral shape. Using the Debye-Scherrer formula, the material’s average crystallite size was found to be 85 nm. Based on the Tauc plot, an optical band gap of the prepared CuO NPs was calculated as 2.6 eV. At room temperature, the material’s magnetic property was investigated using VSM analysis. Congo red was used to examine the photocatalytic properties of the materials with various timings. CuO nanoparticles’ antibacterial activity was evaluated at various doses against Staphylococcus aureus and Klebsiella pneumoniae. Almost, CuO NPs exhibit better response against both the bacteria. Moreover, research investigations using cyclic voltammetry was carried out to assess the produced nanoparticles’ pseudocapacitive qualities. At a scan rate of 10 mV s−1, the material produced a good specific capacitance of 233.8 F/g with 1 M of KOH as an electrolyte.
使用肉豆蔻提取物评估纳米氧化铜的磁性和电化学性能
利用天然提取物合成金属氧化物纳米粒子,可以摆脱危险的有毒物质,从而促进未来环保系统的设计。由于肉豆蔻具有丰富的药用价值,印度的食品工业对肉豆蔻(Myristica fragrans)给予了极大的关注。在本研究中,肉豆蔻水提取物被用来制备纳米氧化铜(CuO)颗粒。植物化学筛选证实了提取物中生物活性物质的存在,如生物碱、甾醇、苷和黄酮类化合物。XRD 和 SEM 测量结果表明,纳米颗粒具有单斜多面体结构。根据 Debye-Scherrer 公式,该材料的平均结晶尺寸为 85 nm。根据陶克曲线图,计算出制备的 CuO NPs 的光带隙为 2.6 eV。在室温下,使用 VSM 分析法研究了材料的磁性。刚果红被用来检测材料在不同时间段的光催化特性。在不同剂量下,评估了 CuO 纳米粒子对金黄色葡萄球菌和肺炎克雷伯氏菌的抗菌活性。结果表明,CuO NPs 对这两种细菌都有较好的抗菌效果。此外,研究人员还利用循环伏安法评估了所制备纳米粒子的假电容特性。在 10 mV s-1 的扫描速率下,以 1 M 的 KOH 作为电解质,该材料产生了 233.8 F/g 的良好比电容。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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