Optimum Green Synthesis, Characterization, and Antibacterial Activity of Silver Nanoparticles Prepared from an Extract of Aloe fleurentinorum

IF 2.3 4区 工程技术 Q3 ENGINEERING, CHEMICAL
Yasmin M. S. Jamil, Ahmed N. Al-Hakimi, Hussein M. A. Al-Maydama, Ghadeer Y. Almahwiti, Ashwaq Qasem, Sayed M. Saleh
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Abstract

The synthesis of metal nanoparticles through the use of plant extract is a process that is not only simple but also inexpensive, quick, and favorable to the environment. As a result, it is utilized in a wide variety of fields. When synthesizing silver nanoparticles (AgNPs), several different kinds of plant extracts were utilized. The manufacture of silver nanoparticles was carried out in this study using an environmentally friendly technique. The aqueous extract of the Aloe fleurentinorum plant was utilized as a stabilizing and reducing agent. To determine the optimal conditions for the synthesis of silver nanoparticles, it was necessary to investigate the impact of several parameters on the process. These parameters included the reactant volume ratio, pH values, temperature, and reaction time. To get crystallite and stable silver nanoparticles, an aqueous solution of AgNO3 (0.01M) was added to an aqueous extract of Aloe fleurentinorum plant at a temperature of 60 degrees Celsius and a pH of 8. The mixture was then stirred with a magnetic stirrer for ninety minutes (90 minutes). Using a variety of methods (UV-vis spectrophotometer, FTIR, XRD, SEM, EDX, and XPS), several approaches were utilized to investigate and describe the green-produced AgNPs. Through the use of the SEM method, it was demonstrated that the morphology of AgNPs is tetrahedral. It was determined using X-ray diffraction that the size of crystalline AgNPs was 26.7 nm. AgNPs that have been optimally synthesized have antibacterial properties that are both significant and effective against various bacterial species that have been tested at varying doses.
用芦荟提取物制备银纳米粒子的最佳绿色合成、表征和抗菌活性
利用植物提取物合成金属纳米粒子的工艺不仅简单,而且成本低廉、速度快、对环境有利。因此,它被广泛应用于各个领域。在合成银纳米粒子(AgNPs)时,使用了几种不同的植物提取物。本研究采用了一种环境友好型技术来制造银纳米粒子。芦荟的水提取物被用作稳定剂和还原剂。为了确定合成银纳米粒子的最佳条件,有必要研究几个参数对合成过程的影响。这些参数包括反应物体积比、pH 值、温度和反应时间。为了得到结晶稳定的银纳米粒子,在温度为 60 摄氏度、pH 值为 8 的条件下,将 AgNO3(0.01M)水溶液加入到芦荟提取物中,然后用磁力搅拌器将混合物搅拌 90 分钟。利用多种方法(紫外-可见分光光度计、傅立叶变换红外光谱、XRD、扫描电镜、EDX 和 XPS)来研究和描述绿色生产的 AgNPs。通过使用扫描电镜方法,证明了 AgNPs 的形态为四面体。利用 X 射线衍射法测定出结晶 AgNPs 的尺寸为 26.7 纳米。经过优化合成的 AgNPs 具有抗菌特性,在不同剂量的测试中,对各种细菌均有显著和有效的抗菌效果。
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来源期刊
International Journal of Chemical Engineering
International Journal of Chemical Engineering Chemical Engineering-General Chemical Engineering
CiteScore
4.00
自引率
3.70%
发文量
95
审稿时长
14 weeks
期刊介绍: International Journal of Chemical Engineering publishes papers on technologies for the production, processing, transportation, and use of chemicals on a large scale. Studies typically relate to processes within chemical and energy industries, especially for production of food, pharmaceuticals, fuels, and chemical feedstocks. Topics of investigation cover plant design and operation, process design and analysis, control and reaction engineering, as well as hazard mitigation and safety measures. As well as original research, International Journal of Chemical Engineering also publishes focused review articles that examine the state of the art, identify emerging trends, and suggest future directions for developing fields.
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