Influence of the extraction method on the chemical, physical and mechanical characteristics of oil palm (Elaeis guineensis) petiole fibers for the reinforcement of composite materials

É. Ze, J. C. Bidoung, W. Nzié, T. Tchotang, B. Kenmeugne
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Abstract

For their use in polymer and composite materials engineering, and with a view to sustainable development, a great deal of work has been carried out with the aim of describing the properties of plant fibers. This work presents the effects of the extraction method on the chemical, physical and mechanical properties of oil palm petiole fibers (OPPF). To this end, the FPPH to be analyzed were obtained by water retting and chemical retting with soda (5% solution). Their physico-chemical and mechanical characteristics were then studied and compared. Fourier transform infrared spectroscopy (FTIR) analysis confirmed the existence of the main components of lignocellulosic fiber (lignin, cellulose and hemicellulose). Lignin was reduced by 22.74%, hemicellulose by 27.33% and cellulose by 16.87% compared to water retting. XRD revealed a crystallinity index of 58.66% for fibers extracted with a 5% sodium solution and 58.51% for fibers extracted with water retting. Soda retting reduces density by 3%. Tensile tests revealed an average tensile strength of 156.082 MPa for water-rubbed fibers and 205.875 MPa for soda-rubbed fibers, Young’s modulus of 3.432 GPa for water-rubbed fibers and 5.346 GPa for soda-rubbed fibers. Elongation at break for FPPH extracted by water retting was 5.178% and 4.41% respectively. This shows that the extraction method affects mechanical properties (flexibility and stiffness) and should be chosen according to the desired characteristic.
提取方法对用于增强复合材料的油棕榈(Elaeis guineensis)叶柄纤维的化学、物理和机械特性的影响
为了将植物纤维应用于聚合物和复合材料工程中,并实现可持续发展,人们开展了大量工作来描述植物纤维的特性。本研究介绍了提取方法对油棕叶柄纤维(OPPF)化学、物理和机械性能的影响。为此,要分析的油棕叶柄纤维是通过水萃取和苏打(5% 溶液)化学萃取获得的。然后对它们的物理化学和机械特性进行了研究和比较。傅立叶变换红外光谱(FTIR)分析证实了木质纤维素纤维主要成分(木质素、纤维素和半纤维素)的存在。与水翻新相比,木质素减少了 22.74%,半纤维素减少了 27.33%,纤维素减少了 16.87%。XRD 显示,用 5% 的钠溶液提取的纤维的结晶度指数为 58.66%,而用水提取的纤维的结晶度指数为 58.51%。苏打水退火使密度降低了 3%。拉伸测试显示,水揉搓纤维的平均拉伸强度为 156.082 兆帕,苏打揉搓纤维的平均拉伸强度为 205.875 兆帕,水揉搓纤维的杨氏模量为 3.432 GPa,苏打揉搓纤维的杨氏模量为 5.346 GPa。用水浸泡提取的 FPPH 断裂伸长率分别为 5.178% 和 4.41%。这表明萃取方法会影响机械性能(柔韧性和刚度),应根据所需的特性进行选择。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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