Xinghui Wang, Yong-jun Cheng, Lian Chen, Meng Dong, Tianyou Feng, Lan Zhao, Ruifang Zhang
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引用次数: 0
Abstract
The core component of a quadrupole mass spectrometer is the quadrupole mass filter, serving a crucial role in ion analysis. It operates by applying two sets of high-voltage, high-frequency signals with equal amplitude and opposing phases through the radio frequency power supply, capitalizing on variations in the electric field and differences in mass-to-charge ratios to separate incoming ions. This study leverages direct digital frequency synthesis technology and multi-stage voltage amplification techniques to design a tailored radio frequency power supply for quadrupole mass spectrometers with a broad mass range. Practical testing demonstrates that this power supply generates radio frequency high-voltage signals with a peak-to-peak voltage ranging from 2.210 V to 4.220 kV at a resonant frequency of 1.240 MHz, facilitating the separation of ions with distinct m/z values. Furthermore, the radio frequency power supply is integrated into a Self-developed quadrupole mass spectrometer, enabling an assessment of the mass range, resolution, stability of the spectrometer. The results of these assessments confirm that the developed power supply accommodates scanning of m/z value ions in the range of 1 to 1067 while maintaining an absolute resolution of less than m/z = 1 units and an instrument stability of 2.00% over four hours.and keywords.
期刊介绍:
Journal of Instrumentation (JINST) covers major areas related to concepts and instrumentation in detector physics, accelerator science and associated experimental methods and techniques, theory, modelling and simulations. The main subject areas include.
-Accelerators: concepts, modelling, simulations and sources-
Instrumentation and hardware for accelerators: particles, synchrotron radiation, neutrons-
Detector physics: concepts, processes, methods, modelling and simulations-
Detectors, apparatus and methods for particle, astroparticle, nuclear, atomic, and molecular physics-
Instrumentation and methods for plasma research-
Methods and apparatus for astronomy and astrophysics-
Detectors, methods and apparatus for biomedical applications, life sciences and material research-
Instrumentation and techniques for medical imaging, diagnostics and therapy-
Instrumentation and techniques for dosimetry, monitoring and radiation damage-
Detectors, instrumentation and methods for non-destructive tests (NDT)-
Detector readout concepts, electronics and data acquisition methods-
Algorithms, software and data reduction methods-
Materials and associated technologies, etc.-
Engineering and technical issues.
JINST also includes a section dedicated to technical reports and instrumentation theses.