Photo-sensitive electrodes based on NiO: SnO2 Nano-composites prepared by chemical method

IF 1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY
H.A.T. Al-ogaili, S. F. Hathot
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Abstract

In the beginning, NiO/SnO2 nanocomposite thin film was prepared of nickel nitrate (1.5213) gm that was weighed and dissolved in distilled water to obtain a specific molar concentration at room temperature and prepared as nanoparticles and mixed with half mount (0.5121) gm of SnO2, in addition to other steps to obtain on the nanocomposite to study some features it. The structural properties of nanocomposite thin films using the chemical technique studied, such as XRD, FE-SEM, and AFM, were found that NiO/SnO2 Nano-composite crystallizes are hexagonal structures with an average crystallite size of 16.30nm. also, the FE-SEM images study the morphology of the NiO: SnO2 thin films, it catches sight of the nanostructure thin films of the NiO: SnO2 Clearly, the surface roughness of nanocomposite according to AFM noted that gets better as a result of the radical’s mobility. The FT-IR spectrum of the synthesized composite has been studied. UV-Spectral absorption of NiO: SnO2 where peak range of wavelength (225-550) nm and notice an increase in the absorption range towards the red wavelength after adding nickel oxide, and use the prepared sample in applied as photosensitive electrodes, voltage characteristics of chemical synthesized: SnO2 nanoparticles shows the current vs voltage plot of chemical-synthesized NiO: SnO2 nanoparticles coated onto glass substrates using dip coating method where add SnO2 due to increasing the conductivity of the nanocomposite.
化学法制备NiO: SnO2纳米复合材料光敏电极
首先,将硝酸镍(1.5213)gm称重,在室温下溶解于蒸馏水中,得到特定的摩尔浓度,制备成纳米颗粒,并与半装量(0.5121)gm的SnO2混合,再通过其他步骤获得纳米复合材料,研究其某些特性。利用化学技术对纳米复合薄膜的结构特性进行XRD、FE-SEM和AFM分析,发现NiO/SnO2纳米复合晶体为六方结构,平均晶粒尺寸为16.30nm。同时,FE-SEM对NiO: SnO2薄膜的形貌进行了研究,发现了NiO: SnO2薄膜的纳米结构,原子力显微镜观察到纳米复合材料的表面粗糙度随着自由基迁移率的提高而提高。研究了合成的复合材料的FT-IR光谱。加入氧化镍后,NiO: SnO2的紫外光谱吸收范围为波长(225-550)nm,并注意到吸收范围向红色波长方向增加,并将制备的样品应用于光敏电极,化学合成的SnO2纳米颗粒的电压特性显示为化学合成的NiO的电流与电压关系图:采用浸涂法将SnO2纳米粒子涂覆在玻璃基板上,其中加入SnO2可以提高纳米复合材料的导电性。
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来源期刊
Digest Journal of Nanomaterials and Biostructures
Digest Journal of Nanomaterials and Biostructures 工程技术-材料科学:综合
CiteScore
1.50
自引率
22.20%
发文量
116
审稿时长
4.3 months
期刊介绍: Under the aegis of the Academy of Romanian Scientists Edited by: -Virtual Institute of Physics operated by Virtual Company of Physics.
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