Synthesis and Characterization of Silver Nanoparticles (AgNPs) using Chemico-physical Methods

Tooba Siddiqui, Mohammad Khalid Zia, Mohammad Muaz, Haseeb Ahsan, Fahim Halim Khan
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Abstract

Silver nanoparticles (AgNPs) have several applications in nanoscience and nanomedicine such as antibacterial, antifungal, anti-inflammatory and anti-angiogenic properties. In the present study, the AgNPs were synthesized by the chemical method and characterised using a combination of UV-Visible (UV-Vis) spectrophotometry, Fourier Transform Infra-Red (FTIR) spectroscopy, transmission electron microscopy (TEM) and X-ray diffraction (XRD). The AgNPs were made by chemically reducing AgNO3 with NaBH4 leading to the formation of a characteristic yellowish-brown colour of AgNPs. To investigate the formation, crystalline behavior, and quality of AgNPs powder, XRD measurements were performed. The produced AgNPs were found to be spherical, dispersed, and scattered in form and the particle size of the AgNPs formed was about 15 nm and they were crystalline in nature. The interaction of AgNO3 with biomolecules may have numerous applications in nanoscience and nanomedicine.
化学物理方法合成银纳米粒子(AgNPs)及其表征
银纳米粒子(AgNPs)在纳米科学和纳米医学中具有多种应用,如抗菌、抗真菌、抗炎和抗血管生成特性。本研究采用化学方法合成了AgNPs,并利用紫外可见分光光度法(UV-Vis)、傅里叶变换红外光谱(FTIR)、透射电子显微镜(TEM)和x射线衍射(XRD)对其进行了表征。AgNPs是用NaBH4化学还原AgNO3制成的,从而形成具有特征的黄褐色AgNPs。为了研究AgNPs粉末的形成、结晶行为和质量,进行了XRD测量。制备的AgNPs呈球形、分散、分散的形态,粒径约为15 nm,呈结晶状。AgNO3与生物分子的相互作用在纳米科学和纳米医学中有着广泛的应用。
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