Impregnation of textile cotton material with Cymbopogon citratus-mediated silver nanoparticles and investigations by light, electron and hyperspectral microscopies

Jean Yves Sikapi Fouda, Agnes Antoinette Ntoumba, Philippe Belle Ebanda Kedi, Thi Hai Yen Beglau, Marcus Fetzer, Till Strothmann, Tchangou Armel Florian, Sone Enone Bertin, Vandi Deli, Emmanuel Jean Teinkela Mbosso, Gustave Leopold Lehman, Emmanuel Albert Mpondo Mpondo, Gisele Etame Loe, Francois Eya’ane Meva, Christoph Janiak
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Abstract

The present study aims to design a cheap and environmentally friendly cotton textile impregnated with green synthesized silver nanoparticles from Cymbopogon citratus leaves. The silver nanoparticles were characterized by umtraviolet spectroscopy and powder X-ray diffraction. Analytical differences between impregnated and non-impregnated cotton textiles were assessed by light, and transmission electron microscopy (TEM). Hyperspectral microscopy reveals the presence of silver nanoparticles inside in situ impregnated cotton material and was coupled to emission spectroscopy to differentiate from cotton fabric giving insight for material quality control. TEM presents high-density dispersions of silver nanoparticles inside the cotton materials and lowest sizes for the in situ impregnated cotton material. The in situ nanomaterial shows differences in maximum emission compared to the cotton fabric, and the particles could be visualized by dark field microscopy. Water and nanoparticle solution retention capacities of the cotton fabrics were determined. The experiment suggests that the in situ impregnated cotton fabric had outstanding washing resistance.
用香茅介导的纳米银浸渍纺织棉材料及其光、电子和高光谱显微镜的研究
本研究旨在设计一种廉价、环保的棉织物,浸渍以香茅叶为原料合成的绿色纳米银。采用紫外光谱和粉末x射线衍射对纳米银进行了表征。用光学和透射电子显微镜(TEM)分析了浸渍棉织物和未浸渍棉织物的分析差异。高光谱显微镜揭示了原位浸渍棉材料中银纳米颗粒的存在,并与发射光谱相结合,以区别于棉织物,从而为材料质量控制提供见解。透射电镜显示,棉材料内部银纳米粒子密度高,而原位浸渍棉材料的粒径最小。与棉织物相比,原位纳米材料显示出最大发射量的差异,并且可以通过暗场显微镜看到颗粒。测定了棉织物的水潴留能力和纳米粒子溶液潴留能力。实验表明,原位浸渍棉织物具有优异的耐水洗性能。
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