Preparation and Characterization of Fe2O3 from Iron Sand of the Coastal Sea of Cidaun Beach-South Cianjur (Indonesia) using the Co-precipitation Method

Q2 Pharmacology, Toxicology and Pharmaceutics
Endah Puspitasari, Masno Ginting, Ramlan Ramlan
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引用次数: 0

Abstract

The synthesis and characterization of Fe2O3 from Iron Sand of the coastal sea of Cidaun Beach - South Cianjur using the coprecipitation method has been carried out. The purpose of this research was to identify the crystal structure, magnetic mineral content, and magnetic properties of iron sands. The characterizations used in this research are X-Ray Diffraction (XRD), Scanning Electron Microscope-Energy Dispersive X-Ray (SEM-EDX) and Vibrating Sample Magnetometer (VSM). Based on the XRD results, it shows that the iron sand sample produces multi-phases, namely hematite (????-Fe2O3), maghemite (????-Fe2O3) and ilmenite (FeTiO3). SEM-EDX results indicate that the iron sand samples have an average particle size of 12.396 ????m. VSM results indicate that the iron sand sample is soft magnetic (ferrimagnetic) with saturation, remanence and coercivity values of 47 emu/g, 1.53 emu/g and 102.97 Oe, respectively.
共沉淀法从Cidaun Beach-South Cianjur (Indonesia)海岸海铁砂中制备Fe2O3及表征
采用共沉淀法,从锡顿海滩-南锡安朱尔海岸的铁砂中合成了Fe2O3并对其进行了表征。本研究的目的是确定铁砂的晶体结构、磁性矿物含量和磁性能。本研究采用x射线衍射(XRD)、扫描电镜-能量色散x射线(SEM-EDX)和振动样品磁强计(VSM)进行表征。XRD结果表明,该铁砂样品存在多相结构,即赤铁矿(????-Fe2O3)、磁铁矿(????-Fe2O3)和钛铁矿(FeTiO3)。SEM-EDX结果表明,铁砂样品的平均粒径为12.396 ????m。VSM结果表明,铁砂样品为软磁(铁磁性),饱和值为47 emu/g,剩磁值为1.53 emu/g,矫顽力值为102.97 Oe。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Science and Technology Indonesia
Science and Technology Indonesia Pharmacology, Toxicology and Pharmaceutics-Pharmacology, Toxicology and Pharmaceutics (miscellaneous)
CiteScore
1.80
自引率
0.00%
发文量
72
审稿时长
8 weeks
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