Tinatin Bukia, Mariam Utiashvili, Manana Tsiskarishvili, Sopo Jalalishvili, Ana Gogolashvili, Tamara Tatrishvili, Gia Petriashvili
{"title":"Synthesis of Some Azo Dyes Based on 2,3,3-Trimethyl-3H-indolenine","authors":"Tinatin Bukia, Mariam Utiashvili, Manana Tsiskarishvili, Sopo Jalalishvili, Ana Gogolashvili, Tamara Tatrishvili, Gia Petriashvili","doi":"10.23939/chcht17.03.549","DOIUrl":null,"url":null,"abstract":"New azo compounds on the base of 2,3,3-trimethyl-3H-indolenine were synthesized and characterized by FT-IR, NMR, and Mas-spectral analysis. The synthesis was conducted in three different pathways: 1) by reducing the nitro compound with Zn/NaOH in alcohol; 2) by heating of 2,3,3-trimethyl-3H-indolenine-5-amine in the presence of MnO2 in toluene, and 3) by diazotization of 2,3,3-trimethyl-3H-indolenine-5-amine and treating the resulting diazonium salt with the appropriate coupler.","PeriodicalId":9762,"journal":{"name":"Chemistry and Chemical Technology","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2023-09-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemistry and Chemical Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.23939/chcht17.03.549","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
New azo compounds on the base of 2,3,3-trimethyl-3H-indolenine were synthesized and characterized by FT-IR, NMR, and Mas-spectral analysis. The synthesis was conducted in three different pathways: 1) by reducing the nitro compound with Zn/NaOH in alcohol; 2) by heating of 2,3,3-trimethyl-3H-indolenine-5-amine in the presence of MnO2 in toluene, and 3) by diazotization of 2,3,3-trimethyl-3H-indolenine-5-amine and treating the resulting diazonium salt with the appropriate coupler.