Characterization of Copper MMC Reinforced with SiC and Graphite in Equal Proportion Made by the Powder Metallurgy Route

Krishna Varma Lanke Rama, Arnuri Srinivasulu, Naidu Gurugubelli Swami, S. Gowtham
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Abstract

Powder metallurgy is playing a very important role in the manufacturing industry. In this research, an attempt is made with copper Metal Matrix Composites (MMC) reinforced with an equal proportion of Silicon Carbide (SiC) and graphite powders. The powders are taken in such a way that the reinforcement weight percentage varies from 0 to 10%. The materials are fabricated through the powder metallurgy route. The powder mixtures are blended and then compacted with a uniaxial pressure of 500 MPa to make the green compacted composites with different compositions. The dimensions of all samples are 25 mm x 16 mm x 16 mm, with an average weight of 40 g. Compacted green samples are sintered by the inert gas sintering process. Sintering is performed at 8000C in an inert argon gas furnace for 120 minutes for all the samples. The obtained samples are made suitable for different tests like porosity, the Vickers hardness test, the wear test, Raman spectroscopy, Scanning Electron Microscopy (SEM), and Energy Dispersive X-Ray (EDX) Analysis. From the values obtained from the hardness test, it is observed that for all MMCs, the minimum value is obtained at Cu-4% (SiC+Gr) and the maximum value at Cu-8% (SiC+Gr), and in between these percentages of composition, there is a little bit of an increase and decrease in values. Wear test results give the maximum wear rate at Cu-4% (SiC+Gr) and the minimum wear rate at Cu-8% (SiC+Gr). Raman spectroscopy test results are given the calculations of Full Width at Half Maximum (FWHM), depth of incident, absorbance, and Id/Ig values, and they are better at 8% of SiC+Gr, which gives the indication of good bonding between molecules of the powder particles. Image analysis is performed using optical microscopy, SEM, and EDX. The microstructures were revealed in such a way that there was good correlation between the properties at different compositions.
粉末冶金法制备等比SiC和石墨增强铜MMC的表征
粉末冶金在制造业中起着非常重要的作用。本研究尝试用等比碳化硅(SiC)和石墨粉增强铜金属基复合材料。粉末采用这样一种方式,即增强重量百分比从0到10%不等。材料采用粉末冶金工艺制备。将粉末混合物混合后,在500 MPa的单轴压力下进行压实,制成不同成分的绿色压实复合材料。所有样品的尺寸为25mm × 16mm × 16mm,平均重量为40g。采用惰性气体烧结工艺烧结压实的绿色试样。所有样品在8000℃的惰性氩气炉中烧结120分钟。所获得的样品适用于不同的测试,如孔隙率,维氏硬度测试,磨损测试,拉曼光谱,扫描电子显微镜(SEM)和能量色散x射线(EDX)分析。从硬度测试值可以看出,所有mmc的硬度值在Cu-4% (SiC+Gr)时最小,在Cu-8% (SiC+Gr)时最大值,在这两个组成百分比之间,硬度值有轻微的增加和减少。磨损试验结果表明,Cu-4% (SiC+Gr)时最大磨损率,Cu-8% (SiC+Gr)时最小磨损率。拉曼光谱测试结果给出了半最大值全宽度(FWHM)、入射深度、吸光度和Id/Ig值的计算结果,在SiC+Gr含量为8%时较好,说明粉末颗粒分子间键合良好。使用光学显微镜,扫描电镜和EDX进行图像分析。显微结构的揭示表明,不同成分下的性能之间存在良好的相关性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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