Radiographic Inspection for Creep Fissures in Reformer-Furnace Tubes

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Abstract

Two steam-methane reformer furnaces were subjected to short-time heat excursions because of a power outage, which resulted in creep bulging in the Incoloy 800 outlet pigtails, requiring complete replacement. Each furnace had three cells, consisting of 112 vertical tubes per cell, each filled with a nickel catalyst. The tubes were centrifugally cast from ASTM A297, grade HK-40 (Fe-25Cr-20Ni-0.40C), heat-resistant alloy. The tube was concluded after metallurgical inspection to have failed from creep rupture (i.e., stress rupture). A project for detecting midwall creep fissuring was instigated as a result of the failure. It was concluded after laboratory radiography and macroexamination that if the fissure were large enough to show on a radiograph, either with or without the catalyst, the tube could be expected to fail within one year. The set up for in-service radiograph examination was described. The tubes of the furnace were radiographed during shut down and twenty-four tubes in the first furnace and 53 in the second furnace showed significant fissuring. Although, radiography was concluded to be a practical technique to provide advance information, it was limited to detecting fissures caused by third-stage creep in tubes because of the cost involved in removing the catalysts.
转化炉管蠕变裂纹的射线检测
由于停电,两台蒸汽-甲烷转化炉发生了短时热偏差,导致incoly 800出口尾辫出现蠕变胀形,需要完全更换。每个熔炉有三个单元,每个单元由112个垂直管组成,每个管中填充镍催化剂。管由ASTM A297离心铸造,等级HK-40 (Fe-25Cr-20Ni-0.40C),耐热合金。经冶金检验,该管因蠕变破裂(即应力破裂)而失效。这次破坏引发了一项检测中壁蠕变裂缝的工程。经过实验室放射线照相和宏观检查后得出结论,如果裂缝大到足以在x光片上显示出来,无论有没有催化剂,管子都可能在一年内失效。介绍了在职x线片检查的设置。停炉时对炉管进行了放射线照相,第一炉24根、第二炉53根管均有明显裂纹。虽然射线照相技术被认为是一种实用的技术,可以提供提前的信息,但由于去除催化剂的成本,它仅限于检测管中第三阶段蠕变引起的裂缝。
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