Fabrication of tungsten micro-rods using electrolyte jet turning method

W. Han, M. Kunieda
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Abstract

The electrolyte jet turning (EJT) method was used to fabricate tungsten micro-rods with the neutral sodium nitrate (NaNO 3 ) aqueous solution as electrolyte. Since the non-conductive oxide film generated on the surface of tungsten interrupts the electrochemical dissolution process, a bipolar current was needed to remove the oxide film during machining. With the bipolar current, sodium hydroxide (NaOH) is generated, when the polarity of the tungsten electrode is negative, enabling the removal of oxide film. A cylindrical nozzle was used for the EJT to jet electrolyte to the surface of workpiece which was rotated with a rotation speed of 3000 rpm. The inner diameter of the cylindrical nozzle determined the diameter of the electrolyte jet, and its influence on the machining characteristics was investigated first. Then, the influences of the duty factor and frequency of pulse voltage on the machining process were investigated to improve the machining accuracy. Finally, tungsten micro-rods with high aspect ratio were fabricated by translating the electrolyte jet on the surface of rod workpiece.
电解液射流车削法制备钨微棒
以中性硝酸钠(nano3)水溶液为电解液,采用电解液射流车削(EJT)法制备钨微棒。由于在钨表面产生的不导电氧化膜中断了电化学溶解过程,因此在加工过程中需要双极电流去除氧化膜。在双极电流下,当钨电极的极性为负时,产生氢氧化钠(NaOH),使氧化膜得以去除。射流喷嘴采用圆柱形喷嘴,以3000转/分的转速将电解液喷射到工件表面。圆柱喷嘴的内径决定了电解液射流的直径,并研究了其对加工特性的影响。为了提高加工精度,研究了脉冲电压占空因数和频率对加工过程的影响。最后,利用电解液射流在钨棒工件表面的平移,制备了高长宽比的钨微棒。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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