High Voltage Plasma Convert Coconut Shell Charcoal To Few Layer Wrinkled Graphene (FLwG)

F. Murdiya, M. R. Epapras, Dede Irawan, A. Hamzah, Firdaus, Suwitno
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Abstract

This research reveals the process of obtaining graphene nanosheets (GNs) by arc discharge with coconut shell (CS) charcoal as base material. The objective research is to convert the CS charcoal powder to graphene nanosheet. The research succeeds to obtain GNs that is few-layer wrinkled graphene (FLwG). FLwG has been produced by burning a coconut-shell-based charcoal by using a plasma arc discharge. Raman spectroscopy and transmission electron microscopy (TEM) were implemented on analyzing of candidate graphene. The arc plasma was supplied in the air gap between the electrodes. The graphite rod was installed as an high voltage electrode and a ground electrode was made of aluminum material. The charcoal powder was put on a ground electrode surface in the air gap of 1.5 cm to the h.v. electrode. It is shown that the Raman spectroscopy analysis indicate an FLwG has been produced. TEM analysis confirms on the presence of FLwG with a wrinkled and folded structure as well. From FTIR analysis, It can be seen that in the FTIR spectrum of the candidate graphene is no significant change associated with the emergence of new characteristic peaks other than the absorption peaks present in the CS Charcoal.
高压等离子体将椰子壳炭转化为几层褶皱石墨烯(FLwG)
研究了以椰子壳炭为基材,采用电弧放电法制备石墨烯纳米片的工艺。研究的目的是将CS炭粉转化为石墨烯纳米片。该研究成功地获得了由少层皱褶石墨烯(FLwG)构成的纳米石墨烯。利用等离子体电弧放电燃烧椰子壳基木炭产生FLwG。利用拉曼光谱和透射电子显微镜对候选石墨烯进行了分析。电弧等离子体在电极之间的气隙中提供。石墨棒安装为高压电极,接地电极由铝材料制成。将炭粉放在与高压电极1.5 cm的气隙处的接地电极表面。拉曼光谱分析表明,产生了FLwG。TEM分析证实了FLwG的存在,并具有褶皱和折叠结构。从FTIR分析中可以看出,在候选石墨烯的FTIR光谱中,除了CS木炭中存在的吸收峰外,没有出现与新的特征峰相关的显著变化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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