Nano edible coatings and films combined with zinc oxide and pomegranate peel active phenol compounds to prolong shelf life of minimally processed pomegranates

Hosam El din Aboul Anean Martirosyan, D. Bader, M. Al-Dossari, N. EL-Gawaad, H. A. Shaat, L. O. Mallasy
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The substances used in this experiment were film with a (A) extract of pomegranate peels (PPE), 5% (0.1%), (B)ZnONPs 1% (0.02%), (C) ZnONPs 2% (0.04%), (D) ZnONPs 3% (0.06%), (E) ZnONPs 1%/PPE1% (0.02%), (F) ZnONPs 2%/PPE2% (0.04%), (G) ZnONPs 3%/PPE3% (0.06%) wt% of chitosan on quality attributes and prolonging the shelf life of pomegranates were stored in edible film containers at 2 °C and 90–95% relative humidity for 20 days. The treatments of (G) ZnONPs 3%/PPE3% (0.06%) loaded on chitosan as well as chitosan and (D) ZnONPs 3% (0.06%) reduced the weight loss, had excellent microbial counts until 20 days of storage, and recorded the lowest microbial count and mold & yeast colonies. Other chemical properties studied included total soluble solids content, acidity, anthocyanin content, firmness, and ascorbic acid. Results indicated that ZnONPs 3%/PPE3% (0.06%) loaded on chitosan or ZnONPs 3% (0.06%) were the best treatments for preserving pomegranate arils. It was found that the best measurements were that the film-forming nano emulsion solutions decreased by E = 110 nm and B = 134 nm. Nano-edibles followed treatment, at F% 188.7 nm, compared to nano-edible films, which were A0% 1312 nm. Background:The substances used in this experiment were film with a (A) extract of pomegranate peels (PPE), 5% (0.1%), (B) ZnONPs 1% (0.02%), (C) ZnONPs 2% (0.04%), (D) ZnONPs 3% (0.06%), (E) ZnONPs 1%/PPE1% (0.02%), (F) ZnONPs 2%/PPE2% (0.04%), (G) ZnONPs 3%/PPE3% (0.06%) wt% of chitosan on quality attributes and prolonging the shelf life of pomegranates were stored in plastic containers at 2 °C and 90–95% relative humidity for 20 days.Objectives: to produce nano-edible films from zinc oxide and active phenol compounds of PPE nanoparticles loaded on chitosan films. The physical and mechanical properties, including viscosity, vapor, zeta particle size emulsion, color, light transmittance, and SEM, were studied to select the best edible coating for improving pomegranate fruit storability under cold storage, as well as minimizing decay and microbial growth during the storage period.Methods:The physical and chemical properties of edible films made with zinc oxide ZnONPs and active phenol compounds extracted from pomegranate peel (PPE) were studied.(A) = PPE extracts, 5% (0.1%) wt% chitosan (B) = ZnONPs, 1% (0.02%) wt% chitosan (C) = ZnONPs, 2% (0.04%) chitosan (D) weight percent = ZnONPs, 3% (0.06%) wt% chitosan weight (E) = ZnONPs 1%/PPE1% (0.02%) 2% ZnONPs/2% PPE (0.04%) Chitosan weight (F) Chitosan weight (G) = ZnONPs 3%/PPE3% (0.06%) Chitosan weight n.s. stands for \"not significantly.\"Results: The treatments of (G) ZnONPs 3%/PPE3% (0.06%) loaded on chitosan as well as chitosan and (D) ZnONPs 3% (0.06%) reduced the weight loss, had excellent microbial counts until 20 days of storage, and recorded the lowest microbial count and mould & yeast colonies. Other chemical properties studied included total soluble solids content, acidity, anthocyanin content, firmness, and ascorbic acid. Results indicated that ZnONPs 3%/PPE3% (0.06%) loaded on chitosan or ZnONPs 3% (0.06%) were the best treatments for preserving pomegranate arils. It was found that the best measurements were that the film-forming nano emulsion solutions decreased by E = 110 nm and B = 134 nm. Nano-edibles followed treatment, at F% 188.7 nm, compared to nano-edible films, which were A0% 1312 nm.Conclusion:Physical and chemical properties were studied, e.g., rheological properties and parathyroid size distribution, zeta potential, and scanning electron microscopy films. Adding nanomaterials to edible coatings prolongs product shelf life, reduces the risk of pathogen growth, and improves the quality of fruit and vegetable surfaces by using low-cost substrates for nano-polymer production to produce edible coatings and film solutions. As this substance inhibits microbial growth and oxidation and improves the quality of the film to preserve the film from oxidation and microbial contamination, maintain the stability of the film, and extend the shelf life of food; acceptable sensory characteristics; appropriate barrier properties (CO2, O2, and water); microbial biochemical and physico-chemical stability; safety and health; and an effective carrier for antioxidants.Keywords: chitosan; ZnONP; pomegranate; mechanical; viscosity; vapor; zeta particle size; color; light transmittance; scanning electron microscopy and Nano-edible Coatings and Films.","PeriodicalId":320142,"journal":{"name":"Dietary Supplements and Nutraceuticals","volume":"3 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-03-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Dietary Supplements and Nutraceuticals","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.31989/dsn.v2i3.1087","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

Abstract

ABSTRACTEdible coating and film from chitosan and incorporating it with the action of ZnONPs on    active phenol compounds from extracts of pomegranate peel (PPE). The physical and chemical properties of edible films made with zinc oxide ZnONPs and active phenol compounds extracted from pomegranate peel (PPE) were studied. Adding ZnONPs with active phenol compounds from extracted pomegranate peel (PPE) to chitosan films can provide safe edible films, decrease microbial growth, consequently, prolong the shelf life of pomegranates, and improve the physiochemical stability of the pomegranate. The substances used in this experiment were film with a (A) extract of pomegranate peels (PPE), 5% (0.1%), (B)ZnONPs 1% (0.02%), (C) ZnONPs 2% (0.04%), (D) ZnONPs 3% (0.06%), (E) ZnONPs 1%/PPE1% (0.02%), (F) ZnONPs 2%/PPE2% (0.04%), (G) ZnONPs 3%/PPE3% (0.06%) wt% of chitosan on quality attributes and prolonging the shelf life of pomegranates were stored in edible film containers at 2 °C and 90–95% relative humidity for 20 days. The treatments of (G) ZnONPs 3%/PPE3% (0.06%) loaded on chitosan as well as chitosan and (D) ZnONPs 3% (0.06%) reduced the weight loss, had excellent microbial counts until 20 days of storage, and recorded the lowest microbial count and mold & yeast colonies. Other chemical properties studied included total soluble solids content, acidity, anthocyanin content, firmness, and ascorbic acid. Results indicated that ZnONPs 3%/PPE3% (0.06%) loaded on chitosan or ZnONPs 3% (0.06%) were the best treatments for preserving pomegranate arils. It was found that the best measurements were that the film-forming nano emulsion solutions decreased by E = 110 nm and B = 134 nm. Nano-edibles followed treatment, at F% 188.7 nm, compared to nano-edible films, which were A0% 1312 nm. Background:The substances used in this experiment were film with a (A) extract of pomegranate peels (PPE), 5% (0.1%), (B) ZnONPs 1% (0.02%), (C) ZnONPs 2% (0.04%), (D) ZnONPs 3% (0.06%), (E) ZnONPs 1%/PPE1% (0.02%), (F) ZnONPs 2%/PPE2% (0.04%), (G) ZnONPs 3%/PPE3% (0.06%) wt% of chitosan on quality attributes and prolonging the shelf life of pomegranates were stored in plastic containers at 2 °C and 90–95% relative humidity for 20 days.Objectives: to produce nano-edible films from zinc oxide and active phenol compounds of PPE nanoparticles loaded on chitosan films. The physical and mechanical properties, including viscosity, vapor, zeta particle size emulsion, color, light transmittance, and SEM, were studied to select the best edible coating for improving pomegranate fruit storability under cold storage, as well as minimizing decay and microbial growth during the storage period.Methods:The physical and chemical properties of edible films made with zinc oxide ZnONPs and active phenol compounds extracted from pomegranate peel (PPE) were studied.(A) = PPE extracts, 5% (0.1%) wt% chitosan (B) = ZnONPs, 1% (0.02%) wt% chitosan (C) = ZnONPs, 2% (0.04%) chitosan (D) weight percent = ZnONPs, 3% (0.06%) wt% chitosan weight (E) = ZnONPs 1%/PPE1% (0.02%) 2% ZnONPs/2% PPE (0.04%) Chitosan weight (F) Chitosan weight (G) = ZnONPs 3%/PPE3% (0.06%) Chitosan weight n.s. stands for "not significantly."Results: The treatments of (G) ZnONPs 3%/PPE3% (0.06%) loaded on chitosan as well as chitosan and (D) ZnONPs 3% (0.06%) reduced the weight loss, had excellent microbial counts until 20 days of storage, and recorded the lowest microbial count and mould & yeast colonies. Other chemical properties studied included total soluble solids content, acidity, anthocyanin content, firmness, and ascorbic acid. Results indicated that ZnONPs 3%/PPE3% (0.06%) loaded on chitosan or ZnONPs 3% (0.06%) were the best treatments for preserving pomegranate arils. It was found that the best measurements were that the film-forming nano emulsion solutions decreased by E = 110 nm and B = 134 nm. Nano-edibles followed treatment, at F% 188.7 nm, compared to nano-edible films, which were A0% 1312 nm.Conclusion:Physical and chemical properties were studied, e.g., rheological properties and parathyroid size distribution, zeta potential, and scanning electron microscopy films. Adding nanomaterials to edible coatings prolongs product shelf life, reduces the risk of pathogen growth, and improves the quality of fruit and vegetable surfaces by using low-cost substrates for nano-polymer production to produce edible coatings and film solutions. As this substance inhibits microbial growth and oxidation and improves the quality of the film to preserve the film from oxidation and microbial contamination, maintain the stability of the film, and extend the shelf life of food; acceptable sensory characteristics; appropriate barrier properties (CO2, O2, and water); microbial biochemical and physico-chemical stability; safety and health; and an effective carrier for antioxidants.Keywords: chitosan; ZnONP; pomegranate; mechanical; viscosity; vapor; zeta particle size; color; light transmittance; scanning electron microscopy and Nano-edible Coatings and Films.
结合氧化锌和石榴皮活性酚化合物的纳米可食用涂层和薄膜,延长最低加工石榴的保质期
摘要壳聚糖制备了可食用的涂层和薄膜,并将其与ZnONPs对石榴皮提取物中活性酚类化合物的作用结合起来。研究了从石榴皮中提取的氧化锌ZnONPs和活性酚类化合物制备可食用薄膜的理化性质。在壳聚糖薄膜中加入含有石榴皮活性酚类化合物的ZnONPs,可以提供安全的食用薄膜,减少微生物的生长,从而延长石榴的保质期,提高石榴的理化稳定性。实验物质为(a)石榴皮提取物(PPE) 5% (0.1%), (B)ZnONPs 1% (0.02%), (C) ZnONPs 2% (0.04%), (D) ZnONPs 3% (0.06%), (E) ZnONPs 1%/PPE1% (0.02%), (F) ZnONPs 2%/PPE2% (0.04%), (G) ZnONPs 3%/PPE3% (0.06%) wt%壳聚糖对石榴品质特性的影响,延长石榴保质期,在2°C, 90-95%相对湿度的可食用薄膜容器中保存20 D。壳聚糖负载(G) ZnONPs 3%/PPE3%(0.06%)处理以及壳聚糖和(D) ZnONPs 3%(0.06%)处理均可减轻体重,在贮藏20 D前微生物数量良好,微生物数量和霉菌菌落最低。研究的其他化学性质包括总可溶性固形物含量、酸度、花青素含量、硬度和抗坏血酸。结果表明,壳聚糖负载ZnONPs 3%/PPE3%(0.06%)或ZnONPs 3%(0.06%)是保存石榴皮的最佳处理。结果表明,成膜纳米乳化液的最佳测量值为E = 110 nm和B = 134 nm。纳米可食用薄膜的F%为188.7 nm,而纳米可食用薄膜的F%为1312 nm。背景:本实验采用(a)石榴皮提取物(PPE) 5% (0.1%), (B) ZnONPs 1% (0.02%), (C) ZnONPs 2% (0.04%), (D) ZnONPs 3% (0.06%), (E) ZnONPs 1%/PPE1% (0.02%), (F) ZnONPs 2%/PPE2% (0.04%), (G) ZnONPs 3%/PPE3% (0.06%) wt%壳聚糖对石榴品质特性的影响,延长石榴在2°C, 90-95%相对湿度的塑料容器中保存20 D。目的:将PPE纳米颗粒的氧化锌和活性酚化合物负载在壳聚糖薄膜上制备可食用纳米薄膜。研究了石榴果实的物理力学性能,包括粘度、水蒸气、zeta粒径、乳化液、颜色、透光率和扫描电镜,以选择最佳的食用涂层,以提高石榴果实的冷藏性,并最大限度地减少贮藏期间的腐烂和微生物生长。方法:对石榴皮(PPE)中氧化锌ZnONPs和活性酚类化合物制备的食用膜的理化性质进行了研究,(A) = PPE提取物,5% (0.1%)wt%壳聚糖(B) = ZnONPs, 1% (0.02%) wt%壳聚糖(C) = ZnONPs, 2%(0.04%)壳聚糖(D)重量百分比= ZnONPs,3% (0.06%) wt%壳聚糖重量(E) = ZnONPs 1%/PPE1% (0.02%) 2% ZnONPs/2% PPE(0.04%)壳聚糖重量(F)壳聚糖重量(G) = ZnONPs 3%/PPE3%(0.06%)壳聚糖重量n.s.表示“不显著”。结果:壳聚糖负载的(G) ZnONPs 3%/PPE3%(0.06%)处理以及壳聚糖和(D) ZnONPs 3%(0.06%)处理均能减轻体重,在贮藏20 D前微生物数量良好,微生物数量和霉菌菌落最低。研究的其他化学性质包括总可溶性固形物含量、酸度、花青素含量、硬度和抗坏血酸。结果表明,壳聚糖负载ZnONPs 3%/PPE3%(0.06%)或ZnONPs 3%(0.06%)是保存石榴皮的最佳处理。结果表明,成膜纳米乳化液的最佳测量值为E = 110 nm和B = 134 nm。纳米可食用薄膜的F%为188.7 nm,而纳米可食用薄膜的F%为1312 nm。结论:研究了其理化性质,如流变学性质、甲状旁腺大小分布、zeta电位、扫描电镜等。将纳米材料添加到可食用涂料中,可以延长产品的保质期,降低病原体生长的风险,并通过使用低成本的基材进行纳米聚合物生产来生产可食用涂料和薄膜溶液,提高水果和蔬菜表面的质量。由于该物质抑制微生物生长和氧化,提高薄膜质量,使薄膜免受氧化和微生物污染,保持薄膜的稳定性,延长食品的保质期;可接受的感官特征;适当的阻隔性能(CO2、O2和水);微生物生化和理化稳定性;安全与健康;也是抗氧化剂的有效载体。 关键词:壳聚糖;ZnONP;石榴;机械;粘度;蒸汽;Zeta粒度;颜色;透光率;扫描电子显微镜和纳米可食用涂层和薄膜。
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