Effect of Heat Treatment on the Oxidation and High Temperature Wear Performance of Alloy Ti-6Al-4V Manufactured by Direct Metal Laser Sintering

R. Shanmugam, Dhinakaran Veeman, Muthu Shanmugam Mannan, Gopika Kalaiselvan
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Abstract

In this work, alloy Ti-6Al-4V was fabricated using direct metal laser sintering (DMLS) approach and studied the effect of heat treatment (solution treatment 950 °C/2h-furnace cooling and aging 550 °C/6h-air cooling) on the oxidation and wear performance at elevated temperature. The microstructural investigation revealed that as-built alloy consists of a fine-grained martensitic needle shape structure with columnar grains. In the solution treatment aging (STA) treated alloy, the rod-shaped β with different lengths of a was observed. As-built and STA-treated alloy Ti-6Al-4V were subjected to a cyclic oxidation test at 650 °C for 50 h in air. The reaction products developed on the sample’s surface are evaluated by scanning electron microscope (SEM) and X-ray diffraction (XRD). A thick TiO2 layer was formed on the alloy surface, and some cracks were noticed due to thermal stress. The high-temperature wear test was carried out on the Ti-6Al-4V alloy at room temperature (30 °C), 200, and 400 °C using a reciprocating pin-on-disc tribometer in dry conditions. The abrasive wear mechanism was found at RT, whereas oxidation and the adhesive mechanism were noticed at 200 and 400 °C. Results exhibited that STA alloy had a higher wear resistance than that of as-built alloy.
热处理对直接金属激光烧结Ti-6Al-4V合金氧化及高温磨损性能的影响
采用直接金属激光烧结(DMLS)法制备了Ti-6Al-4V合金,研究了热处理(固溶处理950°C/2h-炉冷和时效550°C/6h-空冷)对合金高温氧化和磨损性能的影响。显微组织研究表明,铸态合金为细晶马氏体针状柱状组织。在固溶时效(STA)处理合金中,观察到具有不同长度a的棒状β。对Ti-6Al-4V合金在650℃空气中循环氧化50 h。用扫描电子显微镜(SEM)和x射线衍射仪(XRD)对反应产物进行了表征。在合金表面形成了一层较厚的TiO2层,并且由于热应力出现了一些裂纹。在干燥条件下,利用往复式销盘摩擦计对Ti-6Al-4V合金进行了室温(30℃)、200℃和400℃的高温磨损试验。在高温下发现了磨料磨损机制,而在200和400℃时发现了氧化和粘合机制。结果表明,STA合金具有较高的耐磨性。
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