Preparation of CuO Nanorods by Thermal Oxidation in Ozone Ambient

T. Ha, Bach Thanh Cong, P. N. Hai, Nguyễn Hoàng, H. V. Chinh, Bui Thu Huong, N. T. Linh, Bui Truong Son, Tran Thi Quynh Hoa, Tuyen Nguyen Viet
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Abstract

CuO nanorods were prepared by thermal oxidation method in ozone ambient. The effect of annealing temprature in the range from 400 to 600 oC on morphology and structure of nanorods was studied thouroughly by scanning electron microscopy (SEM) and X-ray diffraction, combining with energy dispersive spectroscopy (EDS) and Raman spectroscopy. The results showed that annealing temprature strongly affected the structure and morphology of the produced CuO nanorods. The most uniform nanorods with highest crystal quality were obtained when annealing temperature is from 450 to 500 °C and annealing time was 2 h as suggested by SEM images together with Raman results.
臭氧环境下热氧化法制备氧化铜纳米棒
在臭氧环境下采用热氧化法制备了氧化铜纳米棒。利用扫描电镜(SEM)和x射线衍射,结合能谱(EDS)和拉曼光谱(Raman spectroscopy),深入研究了400 ~ 600℃退火温度对纳米棒形貌和结构的影响。结果表明,退火温度对制备的氧化铜纳米棒的结构和形貌有较大影响。SEM图像和拉曼光谱结果表明,在450 ~ 500℃退火温度和2 h退火时间下,纳米棒的晶粒最均匀,晶体质量最高。
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