E. Rodriguez, L. Ponce, M. Arronte, E. de Posada, G. Kellerman, C. César, L. Barbosa
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引用次数: 1
Abstract
We report the fabrication of glass multilayer doped with semiconductor nanoparticles. The glass matrix was fabricated by Plasma Enhanced Chemical Deposition (PECVD using tetramethoxysilane (TMOS) as precursor. The RF power was supplied by a RF-150 TOKYO HI-Power operating at 13.56 MHz and coupled to the RF electrodes through a matching box. The nanoparticles were grown by pulsed laser deposition (PLD) of a PbTe target using the second harmonic of a Q-Switched Quantel Nd:YAG laser in high purity inert gas atmosphere. The influence of gas and background pressure and in the nanoparticle size and size distribution is studied. The morphological properties of the nanostructured material were studied by means of High Resolution Transmission Electron Microscopy(HRTEM), grazing-incidence smallangleX-ray scattering (GISAXS).
我们报道了掺杂半导体纳米粒子的玻璃多层膜的制备。以四甲基硅烷(TMOS)为前驱体,采用等离子体增强化学沉积(PECVD)法制备了玻璃基体。RF电源由RF-150 TOKYO HI-Power提供,工作频率为13.56 MHz,并通过匹配盒耦合到RF电极上。在高纯惰性气体气氛中,利用调q量子Nd:YAG激光器的二次谐波脉冲激光沉积(PLD) PbTe靶。研究了气体和背景压力对纳米颗粒尺寸和粒径分布的影响。采用高分辨率透射电子显微镜(HRTEM)、掠射小角度x射线散射(GISAXS)研究了纳米结构材料的形态特性。